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Elsevier

Books in Chemistry

Chemistry topic areas include: physical and theoretical, computational, organic, organometallic and inorganic, pharmaceutical and medicinal, analytical and bioanalytical, nuclear, general, nanochemistry, geochemistry, materials and polymer, as well as environmental, green and sustainable chemistry.

  • Separation Processes in the Food and Biotechnology Industries

    Principles and Applications
    • 1st Edition
    • A S Grandison + 1 more
    • English
    This book reviews methods and techniques for separating food components and products of the biotechnology industry. The introduction focuses on food composition and some of the conventional separation techniques. Subsequent chapters deal with each specific type or area of application individually and include information on the basic principles, industrial equipment available, commercial applications and an overview of research and development.

  • The Chemistry of C-Glycosides

    • 1st Edition
    • Volume 13
    • D.E. Levy + 1 more
    • English
    In recent years C-glycoside chemistry has been one of the main topics in carbohydrate chemistry, not only because of the synthetic challenges posed, but also because C-glycosides have the potential to serve as carbohydrate analogues resistant to metabolic processes. Consequently, this class of compounds is currently receiving much interest as a potential source of therapeutic agents for clinical use. This book provides a broad coverage of the various synthetic methods available for the preparation of C-glycosides, and illustrates the interesting breadth of connections between carbohydrate chemistry and modern general synthetic organic chemistry by including topics such as transition-metal catalysis, radical chemistry, cycloaddition and rearrangement processes. In addition, in the final chapter of the book, the syntheses of C-di and trisaccharides reported through 1994 are reviewed. This well organised account of the synthetic chemistry in this field will prove to be very valuable to a wide range of researchers and advanced students, both as an introduction to the topic and for reference.

  • Structure, Fluctuation, and Relaxation in Solutions

    • 1st Edition
    • Volume 83
    • H. Nomura + 2 more
    • English
    The results of a special research project carried out for "Molecular Approaches to Non-equilibrium Process in Solution" were presented during The 42nd Yamada Conference on "Structure, Fluctuation and Relaxation in Solution" which was held from 11-15 December, 1994. The following topics were discussed at the conference:1. Solvation Dynamics 2. Relaxation, Fluctuation and Reaction Dynamics 3. Dynamic Structure and Reaction Mechanisms in Solutions. These topics were the main concern of this conference.

  • Solving Problems with NMR Spectroscopy

    • 1st Edition
    • Atta-ur Rahman + 1 more
    • English
    Solving Problems with NMR Spectroscopy presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving clear examples and solutions. This text will enable organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems to work and the discussion of their solutions and interpretations will help readers becomeproficient in the application of important, modern 1D and 2D NMR techniques to structural studies.

  • Comprehensive Organic Functional Group Transformations

    • 1st Edition
    • Bozzano G Luisa
    • English

  • Advances in Dendritic Macromolecules

    • 1st Edition
    • Volume 2
    • G.R. Newkome
    • English
    The series Advances in Dendritic Macromolecules aims to cover the synthetic, as well as chemical, aspects of this expanding field: the chemistry to and supramolecular chemistry of dendritic or cascade supermolecular compounds. In Chapter 1 of this volume, Hawker and Wooley delineate the convergent growth approach to dendrimers, then relate their three-dimensional architectures to different block polymers. In Chapter 2, Moors and Vögtle describe Professor Vögtle's initial cascade molecules via the repetitive strategy, then expand his original concepts of its application by others, and lastly delineate the synthesis of a new series of tosylamide cascades. They also demonstrate the utility of his original Michael addition/reduction procedure by its application to differ cores. Chapter 3, composed by Professor Engel, describes ionic dendrimers which incorporated an internal transition metal center as well as his work based on ammonium and phosphonium centers. In Chapter 4, Mathias and Carothers review recent studies on silicon-based dendrimers and hyperbranched polymers. Chapter 5, by Kim, describes the preparation and utility of hyperbranched aromatic polymers. Lastly in Chapter 6, Escamilla reviews the historical as well as recent examples of ionic and nonionic bolaamphiphiles.

  • QSAR and Drug Design: New Developments and Applications

    • 1st Edition
    • Volume 23
    • H. Timmerman
    • T. Fujita
    • English
    Based on topics presented at the Annual Japanese (Quantitative) Structure-Activity Relationship Symposium and the Biennial China-Japan Drug Design and Development conference, the topics in this volume cover almost every procedure and subdiscipline in the SAR discipline.They are categorized in three sections. Section one includes topics illustrating newer methodologies relating to ligand-receptor, molecular graphics and receptor modelling as well as the three-dimensional (Q)SAR examples with the active analogue approach and the comparative molecular field analysis. In section 2 the hydrophobicity parameters, log P (1-octanol/water) for compound series of medicinal-chemical interest are analysed physico-organic chemically. Section 3 contains the examples based on the traditional Hansch QSAR approach.A variety of methodologies and procedures are presented in this single volume, along with their methodological philosophies.

  • Advances in Heterocyclic Chemistry

    • 1st Edition
    • Volume 64
    • English
    Established in 1960, Advances in Heterocyclic Chemistry is the definitive serial in the area--one of great importance to organic chemists, polymer chemists, and many biological scientists. Every fifth volume ofAdvances in Heterocyclic Chemistry contains a cumulative subject index.

  • Advances in Food and Nutrition Research

    • 1st Edition
    • Volume 38
    • English
    The appearance of Volume 38 marks a transition for Advances in Food and Nutrition Research as Steve L. Taylor assumes editorial responsibility for the series. Under John Kinsella's guiding hand, Advances in Food Research strengthened its reputation as the leading publication for comprehensive reviews on important topics in food science, evolving into Advances in Food and Nutrition Research, a title which better reflected his interest in the integral relationships between food science and nutrition. Building on this legacy of quality scholarship, Dr. Taylor brings a fresh perspective to the serial, seeking novel approaches to research in food and nutritional science.

  • Optical Spectra and Lattice Dynamics of Molecular Crystals

    • 1st Edition
    • Volume 21
    • G.N. Zhizhin + 1 more
    • English
    The current volume is a single topic volume on the optical spectra and lattice dynamics of molecular crystals. The book is divided into two parts. Part I covers both the theoretical and experimental investigations of organic crystals. Part II deals with the investigation of the structure, phase transitions and reorientational motion of molecules in organic crystals.In addition appendices are given which provide the parameters for the calculation of the lattice dynamics of molecular crystals, procedures for the calculation of frequency eigenvectors of utilizing computers, and the frequencies and eigenvectors of lattice modes for several organic crystals. Quite a large amount of Russian literature is cited, some of which has previously not been available to scientists in the West.

  • Annual Reports in Medicinal Chemistry

    • 1st Edition
    • Volume 30
    • James A. Bristol
    • English
    Praise for the Series:"This series is one of the very few annual publications which justify the title of an absolute must for the pharmacologist, chemist, or physician who is interested in the chemistry of drug development."--Enzym... book is strongly recommended for researchers, teachers, students, administrators - in short, anyone whose interests impinge on medicinal chemistry. In view of the work's documented reference value, it is a must for inlusion in the scientist's personal library."--Journal of Medicinal Chemistry"All topics are covered in sufficient depth, with extensive references, to allow either the specialist or the novice to be informed of the latest developments in a particular area of medicinal chemistry."--Norman Gilman, Hoffmann-La Roche, Inc, in the JOURNAL OF PHARMACEUTICAL SCIENCESAdvances in Medicinal Chemistry continues to provide timely and critical reviews of important topics in medicinal chemistry together with an emphasis on emerging topics in the biological sciences, which are expected to provide the basis for entirely new future therapies.

  • Advances in Physical Organic Chemistry

    • 1st Edition
    • Volume 30
    • English
    The objective of the serial is to present considered reviews on the quantitative study of organic compounds and their behavior--physical organic chemistry in its broadest sense--in a manner accessible to a general readership. This thirtieth volume contains four topics on diverse subjects.

  • Advances in Molecular Structure Research

    • 1st Edition
    • Volume 1
    • English
    Progress in molecular structure research reflects progress in chemistry in many ways. Much of it is thus blended inseparably with the rest of chemistry. It appears to be prudent, however, to review the frontiers of this field from time to time. This may help the structural chemist to delineate the main thrusts of advances in this area of research. What is even more important though, these efforts may assist the rest of the chemists to learn about new possibilities in structural studies, both methodological and interpretation. The aim is to make this a user-oriented series. Structural chemists of excellence will be critically evaluating a field or direction including their own achievements, and charting expected developments.

  • Advances in Inorganic Chemistry

    • 1st Edition
    • Volume 42
    • English
    Advances in Inorganic Chemistry presents timely and informative summaries of the current progress in a variety of subject areas within inorganic chemistry ranging from bio-inorganic to solid state studies. Thisacclaimed serial features reviews written by experts in the area and is an indispensable reference to advanced researchers. Each volume of Advances in Inorganic Chemistry contains an index, and each chapter is fully referenced.

  • Progress in Heterocyclic Chemistry

    A Critical Review of the 1994 Literature Preceded by Two Chapters on Current Heterocyclic Topics
    • 1st Edition
    • Volume 7
    • E. F. V. AAA + 1 more
    • English
    The 16 accounts in Volume 7 are all written by leading researchers in their field and these accounts constitute a systematic survey of the important original material reported in the literature on heterocyclic chemistry in 1994. Chapter 1 surveys useful synthetic routes to "Polyfunctional Pyrroles and Pyrazoles" starting from conjugated azoalkenes. This review is based on the researches of O.A. Attanasi and his school in Urbino (Italy). The second review is unconventional, comprising a compilation of the "Application of Diels-Alder Cycloaddition Chemistry for Heterocyclic Synthesis". Written by the president of the International Society of Heterocyclic Chemistry, A. Padwa, it is in an unusual format, with a pertinent list of references dating back forty years in some cases. The remaining chapters deal with advances in the heterocyclic field, arranged in ascending order or ring size. As with previous volumes in the series, Volume 7 will enable academics and industrial chemists, and advanced students to keep abreast of developments in heterocyclic chemistry in an effortless way.

  • Advances in Heterocyclic Chemistry

    • 1st Edition
    • Volume 63
    • English
    Established in 1960, Advances in Heterocyclic Chemistry is the definitive serial in the area-one of great importance to organic chemists, polymer chemists, and many biological scientists. Every fifth volume ofAdvances in Heterocyclic Chemistry contains a cumulative subject index.

  • Photobiology

    • 1st Edition
    • Elli Kohen + 2 more
    • English
    Photobiology integrates a wide variety of scientific disciplines. As more people become aware of the many ways light interacts with chemical and biological systems, the need for a concise treatment of photobiology has become more critical. Kohen et al. Have written just such a book, intended both as a textbook and as a reference.The authors begin by providing a brief description of the nature of light, how it affects matter, and the means and methods of measuring it. A major section of the book is devoted to how light influences living systems, including discussions of photosynthesis, bioluminescence, regulatory mechanisms, and visual transduction of light. The last half of the book is devoted to the biomedical aspects of light, including photoimmunology, photoallergic reactions and other forms of light sensitivity, the optical properties of skin, and various ways that light can be used in therapy treatments.Useful to photobiologists as a comprehensive overview, this book should also appeal to biomedical researchers and advanced students of photobiology.

  • Adaption of Simulated Annealing to Chemical Optimization Problems

    • 1st Edition
    • Volume 15
    • J.H. Kalivas
    • English
    Optimization problems occurring regularly in chemistry, vary from selecting the best wavelength design for optimal spectroscopic concentration predictions to geometry optimization of atomic clusters and protein folding. Numerous optimization tactics have been explored to solve these problems. While most optimizers maintain the ability to locate global optima for simple problems, few are robust against local optima convergence with regard to difficult or large scale optimization problems. Simulated annealing (SA) has shown a great tolerance to local optima convergence and is often called a global optimizer. The optimizaton algorithm has found wide use in numerous areas such as engineering, computer science, communication, image recognition, operation research, physics, and biology. Recently, SA and variations thereof have shown considerable success in solving numerous chemical optimization problems. The main thrust of this book is to demonstrate the use of SA in a wide range of chemical problems.The potentiality of SA, GSA and other modifications of SA to serve specific needs in a variety of chemical disciplines are covered. A detailed discussion on SA and GSA is given in Chapter 1, presenting the theoretical framework from which a computer program can be written by the reader. The remainder of the book describes applications of SA type algorithms to a diverse set of chemical problems. The final chapter contains an algorithm for GSA written in the MatLab programming environment. This program can be easily adapted to any optimization problem and with only slight modifications, can be altered to perform SA. A general flowchart is also given.

  • Studies in Natural Products Chemistry

    Structure and Chemistry (Part D)
    • 1st Edition
    • Volume 17
    • Atta-ur Rahman
    • English
    Rapid advances in chromatographic procedures, spectroscopic techniques and pharmacological assay methods have resulted in the discovery of an increasing number of new and interesting natural products from terrestrial and marine sources. The present volume contains comprehensive reviews on some of the major advances in this field which have taken place in recent years. The reviews include those on: novel metabolites from marine gastropods; the chemistry of marine natural products of the Halenaquinol family; secondary metabolites from Echinoderms and Bryozoans; triterpenoids and aromatic compounds from medicinal plants; chemistry and activity of sesquiterpenes from the genus Lactarius; the chemistry of bile alcohols; antifungal sesquiterpene dialdehydes; annonaceous acetogenins; nargenicin macrolides; and lignans and diarylheptanoids. Tropane alkaloids and phenolides formed by root cultures are also reviewed. Articles on natural Diels-Alder type adducts, the use of computer aided overlay for modelling the substrate binding domain of HLADH, applications of 170 NMR spectroscopy to natural product chemistry and the role of biological raw materials in synthesis are included. Volume 17 provides material of interest to natural products chemists.

  • Advances in Quantum Chemistry

    • 1st Edition
    • Volume 26
    • English
    Advances in Quantum Chemistry publishes surveys of current developments in the rapidly developing field of quantum chemistry--a field that falls between the historically established areas of mathematics, physics, chemistry, and biology. With invited reviews written by leading international researchers, each presenting new results and insights, this quality serial provides a single vehicle for following progress in this interdisciplinary area.

  • The Chemistry and Pharmacology of Taxol® and its Derivatives

    • 1st Edition
    • Volume 22
    • H. Timmerman
    • V. Farina
    • English
    Taxol®, a naturally occurring diterpenoid is one of the most exciting antitumor drugs available today. Its current indications (refractory ovarian and metastatic breast cancer) may soon be expanded since the drug is showing activity against lung and head-and-neck cancers.The book opens with a review of the naturally occurring taxoids, a chapter which is not a comprehensive list of all taxoids isolated to date, but attempts a systematic approact to describing the different classes of taxoids, with particular reference to all skeletal types and the various functionality patterns. Biosynthetic studies are also discussed, as well as some of the basic chemistry and common functionalities of taxoidic skeleton. Structural identification of taxoids, mostly by spectroscopic means; the formulation of taxanes; the metabolism and pharmacokinetics of Taxol® are also discussed, as are the chemistry of taxanes in relation to SAR studies; SAR aspects of the phenylisoserine side chain; and the mode of action of the taxanes and the mechanisms of resistance.The book is therefore written for medical chemists, in order to stimulate further research in this area and to provide the reader with the necessary background information to start a research program in the area.

  • Advances in Heterocyclic Chemistry

    • 1st Edition
    • Volume 62
    • English
    Established in 1960, Advances in Heterocyclic Chemistry is the definitive serial in the area--one of great importance to organic chemists, polymer chemists, and many biological scientists. Every fifth volume ofAdvances in Heterocyclic Chemistry contains a cumulative subject index.

  • Advances in Atomic Spectroscopy

    • 1st Edition
    • Volume 2
    • J. Sneddon
    • English
    This series describes selected advances in the area of atomic spectroscopy. It is promarily intended for the reader who has a background in atmoic spectroscopy; suitable to the novice and expert. Although a widely used and accepted method for metal and non-metal analysis in a variety of complex samples, Advances in Atomic Spectroscopy covers a wide range of materials. Each Chapter will completely cover an area of atomic spectroscopy where rapid development has occurred.

  • Annual Reports on NMR Spectroscopy

    Special Edition Food Science
    • 1st Edition
    • Volume 31
    • English
    Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry, and pharmaceutics. This volume focuses on theoretical aspects of NMR nuclear shielding and on applications of NMR to polymer science.

  • Spectrophotometry, Luminescence and Colour; Science & Compliance

    • 1st Edition
    • Volume 6
    • Christopher Burgess + 1 more
    • English
    This book contains papers presented at the Second Joint Meeting of the UV Spectrometry Group of the UK and the Council for Optical Radiation Measurements of the USA. Topics included are: compliance and validation in spectrophotometry, advances in spectrophotometric measurements, instrument manufacturers' approaches to compliance, advances in fluorescence techniques and advances in spectrophotometry. The balance of the conference has shifted from the 1986 mix towards more applications but once again the National Laboratories have provided an excellent update on the state-of-the-art in many areas.

  • Heat Exchanger Network Synthesis:

    Process Optimization by Energy and Resource Analysis
    • 1st Edition
    • DR. Uday V. Shenoy Ph.D.
    • English
    Heat Exchanger Network Synthesis provides engineers, designers, and industrial practitioners with a how-to manual for understanding the methodology for conserving energy through process integration.

  • Elements of Statistical Mechanics

    • 3rd Edition
    • D. ter Haar
    • English
    Following the Boltzmann-Gibbs approach to statistical mechanics, this new edition of Dr ter Haar's important textbook, Elements of Statistical Mechanics, provides undergraduates and more senior academics with a thorough introduction to the subject. Each chapter is followed by a problem section and detailed bibliography.The first six chapters of the book provide a thorough introduction to the basic methods of statistical mechanics and indeed the first four may be used as an introductory course in themselves. The last three chapters offer more detail on the equation of state, with special emphasis on the van der Waals gas; the second-quantisation approach to many-body systems, with an examination of two-time temperature-dependen... Green functions; phase transitions, including various approximation methods for treating the Ising model, a brief discussion of the exact solution of the two-dimensional square Ising model, and short introductions to renormalisation group methods and the Yang and Lee theory of phase transitions. In the problem section which follows each chapter the reader is asked to complete proofs of basic theory and to apply that theory to various physical situations. Each chapter bibliography includes papers which are of historical interest. A further help to the reader are the solutions to selected problems which appear at the end of the book.

  • Synthetic Aspects

    • 1st Edition
    • Volume .
    • Philip Page
    • English
    During the last few years, the impact of organosulfur chemistry, especially in the areas of stereocontrolled processes, has led to an explosion of interest in the field. This book is intended to provide in-depth coverage of topics of interest throughout the whole range of organic sulfur chemistry, including bio-organic, physical organic, and synthetic aspects.

  • Biochemical Spectroscopy

    • 1st Edition
    • Volume 246
    • John N. Abelson + 1 more
    • English
    This volume includes spectroscopic methods for the characterization of macromolecules. Methods span the electromagnetic spectrum from X-ray to microwaves. It focuses on the types of information that can be derived: how measurements are made; state of the art apparatus; data acquisition, analysis, and interpretation; casebook examples; and new developments and future directions.

  • Preparation of Catalysts VI

    Scientific Bases for the Preparation of Heterogeneous Catalysts
    • 1st Edition
    • Volume 91
    • G. Poncelet + 4 more
    • English
    The organizers of this Sixth Symposium maintained their initial objectives, namely to gather experts from both industries and universities to discuss the scientific problems involved in the preparation of heterogeneous catalysts, and to encourage as much as possible the presentation of research work on catalysts of real industrial significance. Another highlight of these symposia is to reserve a substantial part of the program to new developments in catalyst preparation, new preparation methods and new catalytic systems. The fact that chemical reactions which were hardly conceivable some years ago have become possible today through the development of appropriate catalytic systems proves that catalysis is in constant progress.The papers in this volume deal with preparation of new catalysts and supports, catalyst preparation via sol-gel methods, supported catalysts and synthesis of nanometer size catalysts.

  • Organomagnesium Methods in Organic Chemistry

    • 1st Edition
    • Basil J. Wakefield
    • English
    The book opens with a general overview of the constitution and reactivity of organomagnesium compounds, followed by information on handling them and on their detection and estimation. Throughout, practical aspects aswell as principles are emphasized. The chapters on the synthesis of organomagnesium compounds cover the preparation of special forms of metallic magnesium and the reaction of magnesium with substrates such as dienes, as well as the traditional preparation of Grignard reagents. Preparations by metallation and metal-halogen exchanges are also included, as are newer methods such as hydromagnesiation of alkenes and alkynes. Systematic coverage is provided on synthetically useful reactions of organomagnesium compounds. Of fundamental importance in organic synthesis are carbon-carbon bond forming reactions; additions to carbon-carbon, carbon-nitrogen, carbon-oxygen, and carbon-sulfur multiple bonds; and nucleophilic substitution at carbon. The formation of carbon-heteroatom bonds in organic compounds is described, where the heteroatom is hydrogen, nitrogen, oxygen, sulfur, or halogen. Finally, the use of organomagnesium compounds in preparing other organometalloid and organometallic compounds is outlined. Representative experimental procedures are included throughout the book, and tables with references to well-described examples are provided.

  • Annual Reports on NMR Spectroscopy

    • 1st Edition
    • Volume 30
    • English
    Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry, and pharmaceutics. This volume focuses on theoretical aspects of NMR nuclear shielding and on applications of NMR to polymer science.

  • Advances in Asymmetric Synthesis

    • 1st Edition
    • Volume 1
    • English

  • Applied Process Design for Chemical and Petrochemical Plants: Volume 1

    • 3rd Edition
    • Ernest E. Ludwig
    • English
    This expanded edition introduces new design methods and is packed with examples, design charts, tables, and performance diagrams to add to the practical understanding of how selected equipment can be expected to perform in the process situation. A major addition is the comprehensive chapter on process safety design considerations, ranging from new devices and components to updated venting requirements for low-pressure storage tanks to the latest NFPA methods for sizing rupture disks and bursting panels, and more.

  • Bioactive Natural Products (Part E)

    V15
    • 1st Edition
    • Volume 15
    • Atta-ur Rahman
    • English

  • Modern Density Functional Theory: A Tool For Chemistry

    • 1st Edition
    • Volume 2
    • P. Politzer + 1 more
    • English
    Density Functional Theory (DFT) is currently receiving a great deal of attention as chemists come to realize its important role as a tool for chemistry. This book covers the theoretical principles of DFT, and details its application to several contemporary problems. All current techniques are covered, many are critically assessed, and some proposals for the future are reviewed. The book demonstrates that DFT is a practical solution to the problems standard ab initio methods have with chemical accuracy.The book is aimed at both the theoretical chemist and the experimentalist who want to relate their experiments to the governing theory. It will prove a useful and enduring reference work.

  • Fortran Programs for Chemical Process Design, Analysis, and Simulation

    • 1st Edition
    • A. Kayode Coker
    • English
    This book gives engineers the fundamental theories, equations, and computer programs (including source codes) that provide a ready way to analyze and solve a wide range of process engineering problems.

  • Retention and Selectivity in Liquid Chromatography

    Prediction, Standardisation and Phase Comparisons
    • 1st Edition
    • Volume 57
    • R.M. Smith
    • English
    This book brings together a number of studies which examine the ways in which the retention and selectivity of separations in high-performance liquid chromatography are dependent on the chemical structure of the analytes and the properties of the stationary and mobile phases. Although previous authors have described the optimisation of separations by alteration of the mobile phase, little emphasis has previously been reported of the influence of the structure and properties of the analyte.The initial chapters describe methods based on retention index group increments and log P increments for the prediction of the retention of analytes and the ways in which these factors are influenced by mobile phases and intramolecular interactions. The values of a wide range of group increments in different eluents are tabulated.Different scales of retention indices in liquid chromatography are described for the comparison of separations, the identification of analytes and the comparison of stationary phases. Applications of these methods in the pharmaceutical, toxicology, forensic, metabolism, environmental, food and other fields are reviewed. The effects of different mobile phases on the selectivity of the retention indices are reported. A compilation of sources of reported retention index values are given.Methods for the comparison of stationary phases based on the interactions of different analytes are covered, including lipophilic and polar indices, shape selectivity comparisons, their application to novel stationary phases, and chemometric methods for column comparisons.

  • Advances in Organobromine Chemistry II

    • 1st Edition
    • Volume 7
    • J.-R. Desmurs + 2 more
    • English
    The organic molecules that are used, particularly in the areas of pharmacy and agrochemicals, are becoming more and more complex both in their chemical nature and spacial configuration. A complex molecular structure is inevitably fragile; it cannot be produced under severe conditions (in particular high pressure and temperature). In addition there is a problem of the scale-up of a product from the laboratory to the industrial scale. The control of the reactivity, selectivity, and yield and the use of sufficiently mild industrial conditions are all factors that must be taken into account by industrial chemists. Amongst the tools giving controllable reactivity, selectivity, and relatively mild reaction conditions is bromine. The organic chemistry of bromine sometimes gives surprising selectivities compared to those of chlorine.This volume which is based on Orgabrom '93, brings together the main contributions presented at this event.

  • Quality Assurance for Environmental Analysis

    Method Evaluation within the Measurements and Testing Programme (BCR)
    • 1st Edition
    • Volume 17
    • E.A. Maier + 2 more
    • English
    Quality assurance (QA) for environmental analysis is a growing feature of the nineties as is illustrated by the number of QA guidelines and systems which are being implemented nowadays. There is, however, often a huge gap between the implementation and respect of QA guidelines and the technical approach undertaken to improve and validate new analytical methods. This is particularly true for complex determinations involving multi-step methodologies such as those used in speciation and organic analyses.Quality assurance may also be considered from the technical point of view, which is the focus of this book. The techniques used in different analytical fields (inorganic, speciation and organic analysis) are critically reviewed (i.e. discussion of advantages and limitations) and existing tools for evaluating their performance are described (e.g. interlaboratory studies, use of certified reference materials). Particular reference is made to the activities of the Measurements and Testing Programme (BCR) of the European Commission towards the improvement of quality control of environmental analysis.The book has been written by experienced practitioners. By its nature, it serves as a practical reference for postgraduate students and environmental chemists who need a wide overview of the techniques used in environmental analysis and existing ways of evaluating the performance of relevant analytical methods. The critical discussions of the methods described, as well as the development of quality assurance aspects, makes it unique.

  • Advances in Detailed Reaction Mechanisms

    Synthetically Useful Reactions
    • 1st Edition
    • James M. Coxon
    • English
    Advances in Detailed Reaction Mechanisms, Volume 4: Synthetically Useful Reactions focuses on synthetically useful reactions, including transition-metal-med... cycloadditions, the use of organoselenium, organozinc, and metal-arene complexes. This book discusses flavonoid synthesis by cyclization of hydrochalcone. Organized into six chapters, this volume begins with an overview of the mechanistic issues related to a number of metal-mediated cycloaddition reactions that are significant in the context of organic synthesis. This text then examines the basic reaction types that generate carbon–carbon bonds. Other chapters consider enzyme and metal-ion-catalyzed isomerization of sugars. This book discusses as well the reaction patterns inherent in polyfunctional organic molecules that are associated with functional groups. The final chapter deals with the nonenzymatic and enzyme-catalyzed-sca... industrial production triggered by commercial applications. This book is a valuable resource for organic synthesis chemists. Scientists and research workers who are interested in synthetically useful reactions will also find this book extremely useful.

  • Quantitative Treatments of Solute/Solvent Interactions

    • 1st Edition
    • Volume 1
    • P. Politzer + 1 more
    • English
    The primary objective of this volume, the first in a new series entitled Theoretical and Computational Chemistry, is to survey some effective approaches to understanding, describing and predicting ways in which solutes and solvents interact and the effects they have upon each other. The treatment of solute/solvent interactions that is presented emphasizes a synergism between theory and experiment. Data obtained experimentally are used as a basis for developing quantitative theoretical models that permit the correlation and interpretation of the data, and also provide a predictive capability. The latter being of course a key motivation for these efforts. Linear solvation energy relationships have been quite successful in this respect and accordingly receive considerable attention. Other effective approaches, including computational ones, are also being pursued, and are discussed in several chapters. This is an area that is continually evolving, and it is hoped that the present volume will convey a sense of its dynamic nature.

  • Lanthanides/Actinides: Physics - II

    • 1st Edition
    • Volume 19
    • G.R. Choppin + 3 more
    • English
    This is the third volume of a three-volume set of reviews devoted to the interrelationships, similarities, differences and contrasts of the lanthanide and actinide series of elements. It comprises five chapters on the comparative physics and thermodynamics of the lanthanide and actinide materials. The first two chapters are concerned with neutron scattering studies, while the next two are concerned with physical property studies involving electronic, thermal and magnetic behaviors. The final chapter covers the thermodynamic properties of metallic systems.The first chapter compares the inelastic neutron scattering behaviours of the lanthanides and actinides. The next chapter concentrates on neutron scattering by heavy fermion single cyrstal materials, including metallic and semiconducting antiferromagnets and nearly insulating paramagnets. Chapter three, probably the most extensive and comprehensive one in the entire series, reviews intermediate valence and heavy fermions in a wide variety of lanthanide and actinide compounds, ranging from metallic to insulating materials. Chapter five focuses on two issues on the high pressure behaviors of anomalous cerium, ytterbium and uranium compounds. The final chapter is an extensive review of the thermodynamic properties of lanthanide and actinide metallic systems.

  • Principles and Practice of Modern Chromatographic Methods

    • 1st Edition
    • Kevin Robards + 2 more
    • English
    Though many separation processes are available for use in todays analytical laboratory, chromatographic methods are the most widely used. The applications of chromatography have grown explosively in the last four decades, owing to the development of new techniques and to the expanding need of scientists for better methods of separating complex mixtures. With its comprehensive, unified approach, this book will greatly assist the novice in need of a reference to chromatographic techniques, as well as the specialist suddenly faced with the need to switch from one technique to another.

  • Chromatography in the Petroleum Industry

    • 1st Edition
    • Volume 56
    • E.R. Adlard
    • English
    Petroleum mixtures consist primarily of relatively unreactive complex hydrocarbons covering a wide boiling range. Such mixtures are difficult to separate by most analytical techniques. Therefore, the petroleum industry has for many years played a leading role in the development of chromatographic methods of analysis. Since the last book specifically concerned with chromatographic analysis of petroleum appeared 15 years ago, numerous advances have been made including developments in liquid and supercritical fluid chromatography, the advent of silica capillary columns with bonded stationary phases and the commercial availability of new selective detectors.The current book contains chapters written by experts concerning the analysis of mixtures ranging from low boiling gases to waxes and crude oils. Silica capillary columns offer excellent resolution but they cannot separate all mixtures; therefore a chapter is devoted to the powerful complementary technique of multidimensional gas chromatography. The analysis of polymers by hydrodynamic chromatography is described as is the analysis of aqueous ionic mixtures by capillary electrophoresis. The atomic emission detector, the oxygen FID and the sulfur chemiluminescence detectors are described and a chapter is devoted to data handling.Although the volume is specifically aimed at the petroleum analyst, there is much information of general interest which should be of benefit to a very wide readership.

  • Carbohydrate Analysis

    High Performance Liquid Chromatography and Capillary Electrophoresis
    • 1st Edition
    • Volume 58
    • Z. El Rassi
    • English
    Carbohydrates and glycoconjugates play an important role in several life processes. The wide variety of carbohydrate species and their inherent polydispersity and heterogeneity require separation techniques of high resolving power and high selectivity such as high performance liquid chromatography (HPLC) and capillary electrophoresis (HPCE). In the last decade HPLC, and recently HPCE methods have been developed for the high resolution and reproducible quantitation of carbohydrates. Despite the importance of these two column separation technologies in the area of carbohydrates, no previous book describes specialized methods for the separation, purification and detection of carbohydrates and glycoconjugates by HPLC and HPCE.Therefore, the objective of the present book is to provide a comprehensive review of carbohydrate analysis by HPLC and HPCE by covering analytical and preparative separation techniques for all classes of carbohydrates including mono- and disaccharides; linear and cyclic oligosaccharides; branched heterooligosaccharid... (e.g., glycans, plant-derived oligosaccharides); glycoconjugates (e.g., glycolipids, glycoproteins); carbohydrates in food and beverage; compositional carbohydrates of polysaccharides; carbohydrates in biomass degradation; etc.The book will be of interest to a wide audience, including analytical chemists and biochemists, carbohydrate, glycoprotein and glycolipid chemists, molecular biologists, biotechnologists, etc. It will also be a useful reference work for both the experienced analyst and the newcomer as well as for users of HPLC and HPCE, graduates and postdoctoral students.

  • Catalyst Design for Tailor-Made Polyolefins

    • 1st Edition
    • Volume 89
    • M. Terano + 1 more
    • English
    Recent development of olefin polymerization catalysts has caused marked changes in both industrial and academic research. Industrial use of homogeneous metallocene catalysts has already begun in the fields of high density polyethylene and syndiotactic polypropylene. Moreover, important data have been obtained from academic investigations which have proved useful for understanding conventional heterogeneous Ziegler-Natta catalysts. From the industrial viewpoint, however, heterogeneous high-yield catalysts seem to be more important.The present volume contains invited lectures and contributed papers. The following topics are covered: (1) Heterogeneous Catalysts, (2) Metallocene Catalysts and (3) New Trends in the Polyolefin Industry.

  • Handbook of Viscosity: Volume 1

    Organic Compounds C1 to C4
    • 1st Edition
    • Carl L. Yaws
    • English
    This series provides engineers with liquid and gas viscosities for the major organic compounds as a function of temperature. The graphs are arranged by chemical formula to provide ease of use; many of them cover the full range from melting point to boiling point to critical point. Common units are used, but each graph displays a conversion factor to provide English units.

  • Annual Reports on NMR Spectroscopy

    • 1st Edition
    • Volume 29
    • English
    Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry, and pharmaceutics. This volume focuses on theoretical aspects of NMR nuclear shielding and on applications of NMR to polymer science.

  • Multidimensional Solid-State NMR and Polymers

    • 1st Edition
    • Klaus Schmidt-Rohr + 1 more
    • English
    NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics.

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