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Books in Nmr spectroscopy

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Solution NMR of Paramagnetic Molecules

  • 1st Edition
  • Volume 2
  • July 4, 2001
  • Ivano Bertini + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 4 1 4 8 - 8
NMR is a growing technique which represents a generalized, spread, common tool for spectroscopy and for structural and dynamic investigation. Part of the field of competence of NMR is represented by molecules with unpaired electrons, which are called paramagnetic. The presence of unpaired electrons is at the same time a drawback (negative effect) and a precious source of information about structure and dynamics. New phenomena and effects are described which are due to the high magnetic fields and advances in the methodology. Solution NMR of Paramagnetic Molecules is unique in dealing with these matters. The scope is that of presenting a complete description, which is both rigorous and pictorial, of theory and experiments of NMR of paramagnetic molecules in solution. Pertinent examples are described. From the time dependent behaviour of electrons in the various metal ions including polimetallic systems to the hyperfine-based information, and from NMR experiments to constraints for solution structure determination. The book's major theme is how to perform high resolution NMR experiments and how to obtain structural and dynamic information on paramagnetic metal ion containing systems.

High-Resolution NMR Techniques in Organic Chemistry

  • 1st Edition
  • Volume 19
  • December 24, 1999
  • T. Claridge
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 0 8 1 2 - 2
From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology.In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

High Resolution NMR

  • 3rd Edition
  • October 4, 1999
  • Edwin D. Becker
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 0 8 0 6 - 1
High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate" level, with mathematics used to augment, rather than replace, clear verbal descriptions of the phenomena. The book is intended to allow a graduate student, advanced undergraduate, or researcher to understand NMR at a fundamental level, and to see illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The presentation is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. Likewise, no previous background in NMR is assumed, since the book begins with a description of the basic physics, together with a brief account of the historical development of the field. This third edition of High Resolution NMR preserves the "conversational" approach of the previous editions that has been well accepted as a teaching tool. However, more than half the material is new, and the remainder has been revised extensively. Problems are included to reinforce concepts in the book.

Annual Reports on NMR Spectroscopy

  • 1st Edition
  • Volume 38
  • June 10, 1999
  • Graham A. Webb
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 8 4 2 1 - 8
Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required, and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry, and pharmaceutics.Once again, the Annual Reports on NMR Spectroscopy represents the best work in the field, both in applied and theoretical NMR spectroscopy. The high calibre reports in Volume 38 show the wide biological and physical applications that benefit from this analytical technique.

Annual Reports on NMR Spectroscopy

  • 1st Edition
  • Volume 37
  • January 13, 1999
  • Graham A. Webb
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 8 4 2 0 - 1
The protean nature of the applications of NMR is regularly reflected in Annual Reports on NMR Spectroscopy. Volume 37 is no exception, and it is an ineluctable fact that all areas of science appear to benefit upon submission to the blandishments of NMR. The examples provided here encompass solid state NMR, solid state NMR imaging, NMR studies of interfaces, NMR investigations of cells and organisms, 199 Mercury NMR, and some applications of NMR to the area of coal science.

Solid State NMR of Polymers

  • 1st Edition
  • Volume 84
  • August 3, 1998
  • T. Asakura + 1 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 4 1 4 6 - 4
In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods.This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described.Features of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists.This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

Annual Reports on NMR Spectroscopy

  • 1st Edition
  • Volume 36
  • May 12, 1998
  • Graham A. Webb
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 8 4 1 9 - 5
This volume has brings together three examples of leading work in the field of NMR Spectroscopy. The contributions show very different applications of spectroscopy, which serve to highlight its importance in an ever increasing number of fields, pure and applied.

Methods for Structure Elucidation by High-Resolution NMR

  • 1st Edition
  • Volume 8
  • December 4, 1997
  • G. Batta + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 3 6 5 0 - 7
Nuclear Magnetic Resonance Spectroscopy (NMR) is now widely regarded as having evolved into a subscience. The field has become immensely diverse, ranging from medical use through solid state NMR to liquid state applications, with countless books and scientific journals devoted to these topics. Theoretical as well as experimental advance continues to be rapid, and has in fact accelerated by many novel innovations. This multi-authored book focuses on the latest developments in the rapidly evolving field of high resolution NMR, specifically with a view to applications on the structure elucidation of organic molecules of moderate molecular weight. Conceptually it differs from basic educational texts, hard-core scientific papers and regular review articles in that each chapter may be regarded as the authors' personal account of their special insights and results that crystallised after several years of research into a given topic. The book revolves around several themes and offers a handful of scientific "gems" of various colors, reflecting the great diversity of NMR. It contains 16 loosely connected chapters written by some of today's most accomplished NMR scientists in the world. Each chapter is a unique synthesis of the authors' previous research results in the given field, and thus projects special insights. Much emphasis has been given to the latest developments in NMR, in particular to selective pulses and pulsed field gradients. As a part of the series "Analytical Spectroscopy Library", with subsequent editions coming along this book should provide a platform for future research accounts of similar flavor. The material is presented in a mostly non-mathematical fashion, and is intended mainly for chemists, application NMR scientists and students with already some background in NMR. Some of the chapters slightly overlap in the discussed topics, which is particularly exciting in terms of gaining insight into the same area from different angles.

Annual Reports on NMR Spectroscopy

  • 1st Edition
  • Volume 34
  • June 24, 1997
  • Graham A. Webb + 1 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 8 4 1 7 - 1
NMR is used in all areas of modern science, and its applications continue to grow. In 1995 we celebrated the 50th anniversary of the discovery of NMR Spectroscopy and almost 30 years since the appearance of the firstvolume of Annual Reports on NMR Spectroscopy. During these years, a large and diverse collection of topics have been covered, and the contents of Volume 34 are no exception. This volume consists of six chapters covering a wide range of polymer science topics. Each chapter demonstrates the unique ability of NMR to provide information of both general and special interests.

NMR Spectroscopy and its Application to Biomedical Research

  • 1st Edition
  • December 4, 1996
  • S.K. Sarkar
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 3 7 5 9 - 7
NMR has become the most diverse spectroscopic tool available to date in biomedical research. It is now routinely used to study biomolecular structure and dynamics particularly as a result of recent developments of a cascade of highly sophisticated multidimensional NMR pulse sequences, and of advances in genetic engineering to produce biomolecules, uniformly or selectively enriched with 13C, 15N and 2H.Features of this book:• Provides an up-to-date treatment of NMR techniques and their application to problems of biomedical interest• Most refined multidimensional pulse sequences including the basic aspects are covered by leading NMR spectroscopists.The book will be useful to NMR spectroscopists, biochemists, and to molecular biologists interested in the use of NMR techniques for solving biological problems.