Books in Spectroscopy

Annual Reports on NMR Spectroscopy

1st Edition
Volume 21
April 24, 1989
Graham A. Webb
English
eBook
9 7 8 0 0 8 0 5 8 4 0 4 1

Commencing with Volume 21, the aim of this series is to produce a larger number of, relatively short but, timely and authoritative reviews. These will concentrate, in particular, on areas of NMR where recent progress, and developments, are of special interest and will reflect the many NMR developments occurring in the primary scientific literature. The present volume demonstrates the advances which can be made by the application of NMR techniques in many diverse areas of chemistry. Of particular significance is the account of Graphics-Aided NMR which will become an inprotant development in the use of NMR spectroscopy.

Analytical Artifacts

1st Edition
Volume 44
January 1, 1989
B.S. Middleditch
English
eBook
9 7 8 0 0 8 0 8 5 8 4 9 4

This encyclopaedic catalogue of the pitfalls and problems that all analysts encounter in their work is destined to spend more time on the analyst's workbench than on a library shelf. The author has dedicated the book to ``the innumerable scientists who made mistakes, used impure chemicals and solvents, suffered the consequences of unanticipated side-reactions, and were otherwise exposed to mayhem yet were not too embarrassed to publish their findings''. Traditionally, the mass spectroscopist or gas chromatographer learnt his trade by participating in a 4-6 year apprenticeship as graduate student and post-doctoral researcher. Generally, no formal training was provided on the things that go wrong, but this information was accumulated by sharing in the experiences of colleagues. Nowadays, many novice scientists simply purchase a computerized instrument, plug it in, and use it. Much time can be wasted in studying and resolving problems due to artifacts and there is also a strong possibility that artifacts will not be recognized as such. For example, most analysts realize that they should use glass rather than plastic containers; but few of them would anticipate the possibility of plasticizer residues on glassware washed using detergent from a plastic bottle.This book is an easy-to-use compendium of problems encountered when using various commonly used analytical techniques. Emphasis is on impurities, by-products, contaminants and other artifacts. A separate entry is provided for each artifact. For specific chemicals, this entry provides the common name, mass spectrum, gas chromatographic data, CAS name and registry number, synonyms and a narrative discussion. More than 1100 entries are included. Mass spectral data are indexed in a 6-peak index (molecular ion, base peak, second peak, third peak) and there are also formula, author and subject indexes. An extensive bibliography contains complete literature citations.The book is designed to be used. It will not only allow experienced analysts to profit from the mistakes of others, but it will also be invaluable to other scientists who use analytical instruments in their work.

Nuclear Magnetic Resonance Spectroscopy

2nd Edition
September 28, 1988
Frank A. Bovey + 2 more
English
eBook
9 7 8 0 0 8 0 9 1 6 9 9 6

Nuclear Magnetic Resonance Spectroscopy, Second Edition focuses on two-dimensional nuclear magnetic resonance (NMR) spectroscopy, high resolution NMR of solids, water suppression, multiple quantum spectroscopy, and NMR imaging. The selection first takes a look at the fundamental principles and experimental methods. Discussions focus on the NMR phenomenon, dipolar broadening and spin-spin relaxation, nuclear electric quadrupole relaxation, saturation, magnetic shielding and chemical shift, magnetic field, transitions between the nuclear energy levels, and resolution and sensitivity considerations. The manuscript then ponders on chemical shift, coupling of nuclear spins, and nuclear relaxation and chemical rate processes. Topics include spin lattice relaxation, spin-spin relaxation, spin decoupling and associated techniques, and description and analysis of spin systems. The text examines two-dimensional NMR spectroscopy, macromolecules, and NMR of solids, including magic angle spinning, cross polarization, proton dipolar broadening, biopolymers, and chain motion in macromolecules. The selection is a valuable source of data for readers interested in nuclear magnetic resonance spectroscopy.

Nuclear Magnetic Resonance Spectroscopy

2nd Edition
September 28, 1988
Frank A. Bovey + 2 more
English
eBook
9 7 8 0 0 8 0 9 1 6 9 9 6

Pulse Methods in 1D & 2D Liquid-Phase NMR

1st Edition
March 28, 1988
Wallace S. Brey
English
eBook
9 7 8 0 0 8 0 9 1 7 0 3 0

FROM THE PREFACE: Pulse Methods in 1D and 2D Liquid-Phase NMR is written to enable the practicing NMR spectroscopist to understand and apply the varied and powerful new techniques developed in the past few years for obtaining spectra with greatly increased information content and from smaller and smaller samples. The intent is to describe both theory and practice in simple and detailed fashion so that the methods may be critically evaluated and effectively used in any potential application. As methods become more complex they require more instrument time, and it is important to be able to judge whether the investment of this time is justified. It is also essential for the spectroscopist to be in a position to evaluate the capabilities of the instrumentation available, as well as the additional requirements for utilization of particular new methods.The material in this book assumes a knowledge of continuous-wave NMR methods as well as an elementary understanding of the normal pulsed Fourier-transform spectroscopic procedures, together with a knowledge of such related phenomena as the nuclear Overhauser effect. Although much of the treatment is necessarily methematical, this aspect of the presentation has been simplified as much as possible.

Annual Reports on NMR Spectroscopy

1st Edition
Volume 17
July 10, 1986
Graham A. Webb
English
eBook
9 7 8 0 0 8 0 5 8 4 0 0 3

NMR spectroscopy has grown to be a vitally important technique with applications in many areas of science. Annual Reports on NMR Spectroscopy is quickly becoming the source for the latest information on current progress, both experimental and theoretical. Chemists in a variety of disciplines will be interested in this up-to-date, comprehensive series.

Atomic Absorption Spectrometry

1st Edition
Volume 5
January 1, 1986
J.E. Cantle
English
eBook
9 7 8 0 0 8 0 8 7 5 5 3 8

The topic is treated here in a very practical manner. The bulk of the book is concerned with real-life analyses for practising instrumentalists and differs from the literature supplied by manufacturers of atomic absorption instruments in that the methods described can be interpreted using all sorts of hardware, and in that far more chemistry and sample preparation are included.

Annual Reports on NMR Spectroscopy

1st Edition
Volume 16
October 1, 1985
Graham A. Webb
English
eBook
9 7 8 0 0 8 0 5 8 3 9 9 0

The current extent of applications of NMR spectroscopy to molecular problems is indicated by the diversity of the reviews presented in this volume. Dr. H.W.E. Rattle reports on NMR of amino acids, peptides, and proteins, which brings his account in Volume 11A up to date.

Phosphorous-31 NMR

1st Edition
February 1, 1984
David G. Gorenstein
English
eBook
9 7 8 0 0 8 0 9 1 8 4 1 9

Phosphorous-31 NMR: Principles and Applications focuses on the evolution of phosphorus-31 nuclear magnetic resonance (NMR) as a widely applied spectroscopic probe of the structure and dynamics of phosphorus-containin... compounds. The selection first offers information on the principles and empirical observations of phosphorus-31 chemical shifts and the principles and applications of phosphorus-31 spin-spin coupling constants. Discussions focus on introduction and basic principles, directly bonded phosphorus coupling constants, and two-bond and three-bond coupling constants. The text then ponders on phosphorus-31 NMR of enzyme complexes and paramagnetic probes of enzyme complexes with phosphorus-containin... compounds. The manuscript elaborates on the use of chiral thiophosphates and the stereochemistry of enzymatic phosphoryl transfer and DNA and RNA conformations. Topics include helix-coil transitions, sequence dependence of double-stranded DNA conformations, dynamic behavior of RNA and DNA, biological and genetic significance, and stereochemical problems studied with chiral thiophosphates. The conformation and dynamics of nucleic acids and phosphoproteins, relaxation behavior of nucleic acids, and theory and applications of solid-state phosphorus-31 NMR to nucleic acids are also discussed. The selection is a valuable reference for readers interested in the principles and applications of phosphorus-31 nuclear magnetic resonance.

Annual Reports on NMR Spectroscopy

1st Edition
Volume 10
April 25, 1980
Graham A. Webb
English
eBook
9 7 8 0 0 8 0 5 8 3 9 1 4

@ISBN@Title@Author@S...

Related subjects

Atomic spectroscopy

Infrared and raman spectroscopy

Laser spectroscopy

Mass spectrometry

Molecular spectroscopy

Nmr spectroscopy

Life Sciences

Physical Sciences & Engineering

Social Sciences & Humanities

Health

Books in Spectroscopy

Annual Reports on NMR Spectroscopy

Analytical Artifacts

Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy

Pulse Methods in 1D & 2D Liquid-Phase NMR

Annual Reports on NMR Spectroscopy

Atomic Absorption Spectrometry

Annual Reports on NMR Spectroscopy

Phosphorous-31 NMR

Annual Reports on NMR Spectroscopy

Related subjects