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Books in Materials analysis and characterization

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Thermally Activated Mechanisms in Crystal Plasticity

  • 1st Edition
  • Volume 8
  • September 8, 2003
  • D. Caillard + 1 more
  • English
  • Hardback
    9 7 8 - 0 - 0 8 - 0 4 2 7 0 3 - 4
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 4 2 7 8 - 2
KEY FEATURES:A unified, fundamental and quantitative resource. The result of 5 years of investigation from researchers around the worldNew data from a range of new techniques, including synchrotron radiation X-ray topography provide safer and surer methods of identifying deformation mechanisms Informing the future direction of research in intermediate and high temperature processes by providing original treatment of dislocation climb DESCRIPTION:Thermally Activated Mechanisms in Crystal Plasticity is a unified, quantitative and fundamental resource for material scientists investigating the strength of metallic materials of various structures at extreme temperatures. Crystal plasticity is usually controlled by a limited number of elementary dislocation mechanisms, even in complex structures. Those which determine dislocation mobility and how it changes under the influence of stress and temperature are of key importance for understanding and predicting the strength of materials. The authors describe in a consistent way a variety of thermally activated microscopic mechanisms of dislocation mobility in a range of crystals. The principles of the mechanisms and equations of dislocation motion are revisited and new ones are proposed. These describe mostly friction forces on dislocations such as the lattice resistance to glide or those due to sessile cores, as well as dislocation cross-slip and climb. They are critically assessed by comparison with the best available experimental results of microstructural characterization, in situ straining experiments under an electron or a synchrotron beam, as well as accurate transient mechanical tests such as stress relaxation experiments. Some recent attempts at atomistic modeling of dislocation cores under stress and temperature are also considered since they offer a complementary description of core transformations and associated energy barriers.In addition to offering guidance and assistance for further experimentation, the book indicates new ways to extend the body of data in particular areas such as lattice resistance to glide.

Characterization of Porous Solids VI

  • 1st Edition
  • Volume 144
  • November 14, 2002
  • F. Rodríguez-Reinoso + 3 more
  • English
  • Hardback
    9 7 8 - 0 - 4 4 4 - 5 1 2 6 1 - 1
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 8 9 1 - 5
This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002. Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

Microscopy Techniques for Materials Science

  • 1st Edition
  • October 29, 2002
  • A Clarke + 1 more
  • English
  • eBook
    9 7 8 - 1 - 8 5 5 7 3 - 7 5 0 - 1
This comprehensive reference work provides an overview of, and practical guide to, the various computer-aided microscopical techniques used in materials science today. After introducing the reader to the basic concepts of optics, the interactions between light and matter, and image processing, the book goes on to discuss in depth both 2D reflection microscopy and confocal laser scanning microscopy. The application of these techniques to the characterisation of materials is abundantly illustrated by hundreds of photographs and illustrations, and through specific case studies. There is also discussion of other modern optical imaging techniques and of non-optical ones such as x-ray micrography. This reference text is essential both for beginners looking for an introduction to the subject as well as advanced materials researchers in the fields where optical microscopy is used.

The Porphyrin Handbook

  • 1st Edition
  • July 31, 2002
  • Karl Kadish + 2 more
  • English
  • Hardback
    9 7 8 - 0 - 1 2 - 3 9 3 2 2 6 - 6
  • eBook
    9 7 8 - 0 - 0 8 - 0 9 2 3 9 0 - 1
The Porphyrin Handbook, Volume 16: Phthalocyanines: Spectroscopic and Electrochemical Characterization provides information pertinent to every aspect of the chemistry, synthesis, spectroscopy, and structure of phthalocyanines. This book examines the biology and medical implications of porphyrin systems. Organized into five chapters, this volume begins with an overview of the photophysical properties of phthalocyanines that are important in relation to photosensitizers in photodynamic therapy, photoconductor, solar cells, and artificial photosynthesis. This text then describe how the data obtained from magnetic circular dichroism spectroscopy has provided the critical information required to describe the excited and ground state degeneracies of main group metallophthalocyanines complexes. Other chapters consider the electrocatalysis by electrodes modified with phthalocyanine sensors and complexes. This book discusses as well the properties of phthalocyanines and of their complexes. The final chapter deals with the experiments with organic pigment thin films. This book is a valuable resource for research scientists, engineers, and clinicians.

Handbook of Elastic Properties of Solids, Liquids, and Gases, Four-Volume Set

  • 1st Edition
  • October 23, 2000
  • Moises Levy + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 9 2 4 2 5 - 0
Sound waves propagate through galactic space, through two-dimensional solids, through biological systems, through normal and dense stars, and through everything that surrounds us; the earth, the sea, and the air. We use sound to locate objects, to identify objects, to understand processes going on in nature, to communicate, and to entertain. The elastic properties of materials determine the velocity of sound in them and tell us about their response to stresses something which is very important when we are trying to construct, manufacture, or create something with any material. The Handbook of Elastic Properties of Materials will provide these characteristics for almost everything whose elastic properties has ever been measured or deduced in a concise and approachable manner.Leading experts will explain the significance of the elastic properties as they relate to intrinsic microscopic behavior, to manufacturing, to construction, or to diagnosis. They will discuss the propagation of sound in newly discovered or created materials, and in common materials which are being investigated with a fresh outlook.The Handbook will provide the reader with the elastic properties of the common and mundane, the novel and unique, the immense and the microscopic, and the exhorbitantly dense and the ephemeral.. You will also find the measurement. And theoretical techniques that have been developed and invented in order to extract these properties from a reluctant nature and recalcitrant systems.

New Carbons - Control of Structure and Functions

  • 1st Edition
  • April 20, 2000
  • Michio Inagaki
  • English
  • Hardback
    9 7 8 - 0 - 0 8 - 0 4 3 7 1 3 - 2
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 5 7 0 - 9
The discovery of fullerenes and nanotubes has greatly stimulated the interest of scientists and engineers in carbon materials, and has resulted in much scientific research. These materials have provided us with many interesting ideas and potential applications, some of them practical and some simply dreams for the future. In the early 1960s, carbon fibers, glass-like carbons and pyrolytic carbons were developed which were quite different from the carbon materials that had previously been used. Carbon fibers exhibited surprisingly good mechanical properties, glass-like carbons exhibited brittle fracture resulting in a conchoidal fracture surface similar to sodium glass, and giving no carbon dust, and pyrolytic carbons were produced by a new production process of chemical vapour deposition and showed very high anisotropy. These carbons materials made a great impact not only on the carbon community who had been working on carbon materials but also on people working in the fields of materials science and engineering. They were used to develop a variety of new applications in technological fields, such as semiconductors, microelectronics, aerospace and high temperature, etc. These newly developed carbon materials were called NEW CARBONS, in comparison with carbon materials such as artificial graphites represented by graphite electrodes, carbon blacks and activated carbons, which maybe thought of as CLASSICAL CARBONS. Later, other new carbons, such as activated carbons and those with novel functions, isotropic high-density graphites, intercalation compounds, various composites, etc., were developed. In 1994, Professor Michio Inagaki published a book entitled "New Carbon Materials — Structure and Functions" with his friend Professor Yoshihiro Hishiyama of Musashi Institute of Technology, published by Gihoudou Shuppan in Japanese. However, progress in the fields of these new carbons is so rapid that the previous book is already out of date. For this reason the author has decided to write an English text on New Carbons. The text focuses on New Carbons based on hexagonal networks of carbon-atoms, i.e. graphite-related materials. The fundamental concept underlying this book is that the structure and functions of these materials are principally governed by their texture. The aim is to give readers a comprehensive understanding of New Carbons through the description of their structure and texture, along with the properties that are largely dependent on them.

Ceramics and Ceramic Composites

  • 1st Edition
  • December 14, 1999
  • G. Elssner + 3 more
  • English
  • Hardback
    9 7 8 - 0 - 4 4 4 - 1 0 0 3 0 - 6
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 8 8 1 - 6
Ceramics and ceramic composites are now used in almost all areas of technology and have potential for even greater and more widespread applications. To make this a reality, it is increasingly necessary to understand the microstructure of the material and its relationship with properties and performance. Central to this is the characterization of the material, in particular using optical and scanning electron microscopy techniques.This book acts as an expert guide to the various steps necessary for successful and accurate characterization of these materials including the crucially important preparation stage, the techniques used to reveal the microstructure and the analysis of the results.In particular, the book presents fundamental information on preparing polished sections of ceramics and ceramic composites including the main steps of sampling, sectioning, mounting and impregnation, and mechanical grinding, lapping and polishing. It discusses microstructural imaging in the optical microscope (OM) and the use of the scanning electron microscope (SEM). Etching or contrast enhancement following final polishing in order to reveal the material's microstructure is also covered.An entire chapter is devoted to material-specific preparation procedures for polished sections. These procedures take into account the properties of the ceramic or composite being examined and the purpose of the examination. They have proven to be very suitable for the respective materials and are effective for revealing the pores. The examples presented here for ceramics and ceramic composites provide polished sections of good to excellent quality for routine examination under the optical microscope. They include tips for etching and contrast enhancement, as well as microstructural images. Chapter 5 discusses the preparation of polished sections for purposes of examination and contains information on producing oblique sections and controlled removal of material. It also addresses the production of thin sections. As a complement to the examination of the microstructure, chapter 6 provides insight into the evaluation of hardness testing indentations. Chapter 7 concludes this work with an overview of the technical literature.

Thermophysical Properties of Materials

  • 1st Edition
  • September 22, 1999
  • G. Grimvall
  • English
  • Hardback
    9 7 8 - 0 - 4 4 4 - 8 2 7 9 4 - 4
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 4 2 8 6 - 7
This is a thoroughly revised version of the original book published in 1986. About half of the contents of the previous version remain essentially unchanged, and one quarter has been rewritten and updated. The rest consists of completely new and extended material. Recent research has focussed on new materials made through "molecular engineering", and computational materials science through ab initio electron structure calculations. Another trend is the ever growing interdisciplinary aspect of both basic and applied materials science. There is an obvious need for reviews that link well established results to the modern approaches. One purpose of this book is to provide such an overview in a specific field of materials science, namely thermophysical phenomena that are intimately connected with the lattice vibrations of solids. This includes, e.g., elastic properties and electrical and thermal transport. Furthermore, this book attempts to present the results in such a form that the reader can clearly see their domain of applicability, for instance if and how they depend on crystal structure, defects, applied pressure, crystal anisotropy etc. The level and presentation is such that the results can be immediately used in research. Graduate students in condensed matter physics, metallurgy, inorganic chemistry or geophysical materials will benefit from this book as will theoretical physicists and scientists in industrial research laboratories.

Microstructural Characterisation of Fibre-Reinforced Composites

  • 1st Edition
  • July 10, 1998
  • John Summerscales
  • English
  • eBook
    9 7 8 - 1 - 8 5 5 7 3 - 7 5 6 - 3
Over the last 50 years, great progress has been made in developing artificial fibre-reinforced composite materials, generally using filaments with microscopic diameters. A wide range of reinforcement forms, from random arrays to fully aligned, can be used for commercial applications, with the microstructure being a critical factor in realising the required properties in a material.This is the first up-to-date review of how to apply advanced microstructural characterisation techniques to fibre-reinforced composites. Each chapter is designed to offer both a stand-alone introduction to its topic and detailed referencing for follow-up research. With contributions from experts from around the world, the book will be an essential reference for materials scientists and research workers in industry and academia alike.

Dynamics of Thin Walled Elastic Bodies

  • 1st Edition
  • October 6, 1997
  • J. D. Kaplunov + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 0 4 8 6 - 5
Written by a well-known group of researchers from Moscow, this book is a study of the asymptotic approximations of the 3-D dynamical equations of elasticity in the case of thin elastic shells of an arbitrary shape. Vibration of shells is a very useful theory in space techniques, submarine detection, and other high-tech domains. Dynamics of Thin Walled Elastic Bodies shows that refined shell theories used in engineering practice give a distorted picture of the high-frequency or non-stationary dynamics of shells, and offers new, mathematically more consistent ways of describing the dynamics of shells.