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Books in Analytical separations

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Special Distillation Processes

  • 1st Edition
  • February 22, 2005
  • Zhigang Lei + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 4 5 5 7 5 - 4
Special distillation processes are required for separation of mixtures close to boiling point or for forming azeotrope mixtures into their pure components. In Special Distillation Processes, the authors focus on latest developments in the field, such as separation methods that may prove useful for solving problems encountered during research. Topics include extraction, membrane and adsorption distillation involving the separation principle, process design and experimental techniques. The relationship between the processes and the techniques are also presented. Comprehensive and easy-to-read, this book provides key information needed to understand the processes and is a valuable reference source for chemical engineers as well as students wishing to branch out in chemical engineering.

Interfacial Separation of Particles

  • 1st Edition
  • Volume 20
  • January 25, 2005
  • Shouci Lu + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 4 9 5 4 5 - 3
Interfacial Separation of Particles is concerned with the processing and separation of fine solid particles in liquid solutions using interfacial technology.Interfacial separation has been finding wide application in many industrial fields, such as pigment and filler production, mineral processing, environmental protection, hydrometallurgy, bioengineering, food and beverage industry and chemical industry. This book describes all interfacial separation techniques and discusses the general and specific fundamentals of the techniques. The book intends to promote theoretical understanding and the more promising developments of interfacial separation technology whilst broadening the reader's background knowledge of industrial suspensions.

Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

  • 1st Edition
  • Volume 43
  • December 11, 2004
  • A.R. Fernandez Alba
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 4 5 4 4 0 - 5
The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects.

Chromatography

  • 6th Edition
  • Volume 69B
  • April 16, 2004
  • E. Heftmann
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 4 7 2 2 5 - 6
Chromatography has emerged as the most important and versatile analytical method. The book is not only an updated version of Heftmann's classical text, but it covers areas of future importance, such as microfluidics and computer resources. Under his experienced guidance, authorities in each field have contributed their practical experience to an integrated treatment of modern micro analysis. Part B of this two volume set brings the traditional field of application up to date. These include amino acids and proteins, nucleic acids and their constituents, lipid, and carbohydrates. Special chapters are devoted to the most important areas of application: drug and environmental analysis. Forensic and phytochemical applications are covered for the first time. Together with an overview of computer resources, the subject index allows novices as well as experts to obtain rapid and authoritative guidance to analytical problems, such as choice of methods and optimization of techniques and instrumentation.

Bioanalytical Separations

  • 1st Edition
  • Volume 4
  • September 3, 2003
  • Ian D. Wilson
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 7 8 6 - 4
Bioanalytical Separations is volume 4 of the multi-volume series, Handbook of Analytical Separations, providing reviews of analytical separation methods and techniques used for the determination of analytes across a whole range of applications. The theme for this volume is bioanalysis, in this case specifically meaning the analysis of drugs and their metabolites in biological fluids.

Sampling and Analysis of Environmental Chemical Pollutants

  • 1st Edition
  • July 8, 2003
  • E. P. Popek
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 4 7 4 3 0 - 4
An excellent introduction to the real world of environmental work, this title helps both college students and working professionals improve their understanding of the data collection process. It covers all phases of data collection (planning, field sampling, laboratory analysis, and data quality assessment), and is a single source comprehensive reference for the resolution of the most common problems that environmental professionals face daily in their work. Why This TitleThis title is written in a clear and logical manner that is accessible to environmental professionals of all disciplines. It contains hundreds of practical tips on planning, sampling, and interactions with analytical laboratories. Having this text as a desk reference will greatly improve skills in planning and sampling, and elevate understanding of chemical data to a new level. This topic is of importance to a wide range of environmental professionals from a variety of disciplines (see audience). Written by a practicing professional for practicing professionals, this handbook provides everything an environmental professional needs to know to competently collect environmental chemical data.

Monolithic Materials

  • 1st Edition
  • Volume 67
  • April 29, 2003
  • F. Svec + 2 more
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 3 6 9 7 - 2
During the past decade, monolithic materials in the shape of discs, stacked layers, rolled sheets, sponges, irregular chunks, tubes, and cylinders have all been successfully demonstrated. These formats were prepared from a wide variety of materials including natural polymers such as cellulose, synthetic polymers that involved porous styrene-, methacrylate-, and acrylamide-based polymers, and inorganic materials, mainly silica. Each approach is interesting from the point of view of both preparation and application.Although the current papers and patents concerned with monolithic separation media are quite numerous, the information is scattered throughout a vast number of journals. This book therefore fills the gap in the market for a comprehensive reference book on this subject.Monolithic materials concerns all of the current formats of monolithic materials and provides an integrated view of this novel format of separation media. Since the flow pattern in monolithic devices is different from that in packed beds, the hydrodynamics of the system and mass transport differ considerably from those derived for packed columns. Therefore, this book presents contributions concerned with both flow and mass transfer in the monolithic materials. A significant proportion of the book is devoted to the applications of monolithic materials. It also provides the reader with valuable information about the sources of the specific materials, their properties, and potential applications.

Carbohydrate Analysis by Modern Chromatography and Electrophoresis

  • 1st Edition
  • October 31, 2002
  • Ziad El Rassi
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 8 4 9 - 6
This book is an updated and expanded edition of Carbohydrate Analysis, High Performance Liquid Chromatography and Capillary Electrophoresis and is concerned with the analysis of carbohydrates by modern chromatography and electrophoresis including analytical and preparative high performance liquid chromatography (HPLC), thin layer chromatography (TLC), field flow fractionation (FFF), capillary electrophoresis (CE), capillary electrochromatography (CEC), polyacrylamide gel electrophoresis (PAGE), gas chromatography (GC) and supercritical fluid chromatography (SFC). Thirty-one chapters cover: various modes of HPLC, CE, CEC, FFF, GC and SFC that are currently applied to the analysis of carbohydrates; discussions on analytical and preparative separations; descriptions of the principles of detection and quantitative determination of carbohydrates by the various separation techniques; reviews of sample preparations; and information on important applications. Furthermore, the book describes in detail the different direct and indirect detection methods that have been introduced for the sensitive detection of carbohydrates. This title is useful for a wide audience including separation scientists; analytical chemists and biochemists; carbohydrate chemists; glycoprotein and glycolipid chemists; molecular biologists; and biotechnologists. The book is also a useful reference for both the experienced analyst and the newcomer and for users of modern chromatography and electrophoresis.

Countercurrent Chromatography

  • 1st Edition
  • Volume 38
  • October 10, 2002
  • A. Berthod
  • English
  • eBook
    9 7 8 - 0 - 0 8 - 0 9 2 9 6 6 - 8
Countercurrent chromatography (CCC) is a separation technique in which the stationary phase is a liquid. The mobile phase is also a liquid, so biphasic liquid systems with at least two solvents are used. Centrifugal fields are used to hold the liquid stationary phase while pushing the liquid mobile phase through it.This comprehensive reference covers recent advancements in the two types of CCC machines: the high speed CCCs without rotary seals and with coiled spools and centrifugal partition chromatographs (CPC) with rotary seals and interconnected channels. Written by leading international experts in the CCC field, the book focuses on the liquid nature of the stationary phase: giving newcomers the basis to do CCC efficiently and rapidly; explaining the art of obtaining a biphasic liquid system; describing the flow patterns in both CPC and high speed CCC machines; showing possible other uses of a liquid stationary phase; presenting a wealth of applications in the separation of organic, pharmaceutical and inorganic mixtures; and demonstrating that even supercritical fluids can be used in CCC.

Acceleration and Automation of Solid Sample Treatment

  • 1st Edition
  • Volume 24
  • August 9, 2002
  • J.L. Luque García + 1 more
  • English
  • Hardback
    9 7 8 - 0 - 4 4 4 - 5 0 7 1 6 - 7
  • eBook
    9 7 8 - 0 - 0 8 - 0 5 2 5 8 6 - 0
This book aims to provide scientists with information about a series of techniques that can be used with a view to facilitating the transformation of the sample to an appropriate state for subsequent detection or quantitation of its components of interest. The techniques dealt with range from the very simple ones (e.g. freeze-drying) to other more complex ones (e.g. glow discharge and laser-induced breakdown sampling). This is the first compilation ever on the subjects of acceleration of solid sample pretreatment; automation of solid sample pretreatment; and integration of solid sample pretreatment and detection. Readers will find here the information required to compare and select the best choice for each sample treatment need and ways to facilitate or automate the most complex and time-consuming step of the analytical process when solid samples are involved.