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Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods
- 1st Edition, Volume 1 - December 2, 2012
- Authors: J.T. Clerc, E. Pretsch, J. Seibl
- Language: English
- eBook ISBN:9 7 8 - 0 - 4 4 4 - 5 9 7 5 4 - 0
Structural Analysis of Organic Compounds covers some practical analytical aspects of organic structural analysis by combined application of spectroscopic methods. This book is… Read more
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Request a sales quoteStructural Analysis of Organic Compounds covers some practical analytical aspects of organic structural analysis by combined application of spectroscopic methods. This book is composed of three parts encompassing 35 chapters that specifically describe infrared-, ultraviolet-, proton and carbon-13 nuclear magnetic resonance and mass spectroscopy. Considerable chapters discuss the problems intended to cover a wide variety of chemical structure and spectroscopic argument, thereby exemplifying interpretations and comment on specific practical aspects of the problem solving procedure. The remaining chapters provide short supplementing research concerning various aspects of structural analysis. This book will prove useful to organic and analytical chemists.
PrefacePart 1 Initial Remarks Presentation of Data Mass Spectra Infrared Spectra Proton NMR Spectra Carbon-13 NMR Spectra Ultraviolet Spectra Assisting Measures Mass Spectroscopy Infrared Spectroscopy Proton NMR Spectroscopy Carbon-13 NMR Spectroscopy Ultraviolet Spectroscopy Reference Data Combined Tables for All Methods Used in this Context Mass Spectroscopy Infrared Spectroscopy Proton NMR Spectroscopy Carbon-13 NMR Spectroscopy Ultraviolet Spectroscopy Technical Terms Isochronous Nuclei Magnetic Equivalence Nomenclature of Spin Systems Working PhilosophyPart 2 Problems Problem 1 Elemental Composition and Structural Features Structural Assembly Comments Problem 2 Elemental Composition and Structural Features Structural Assembly Comments Problem 3 Elemental Composition and Structural Features Structural Assembly Comments Problem 4 Elemental Composition and Structural Features Structural Assembly Comments Problem 5 Elemental Composition and Structural Features Structural Assembly Comments Problem 6 Elemental Composition and Structural Features Structural Assembly Comments Problem 7 Elemental Composition and Structural Features Structural Assembly Comments Problem 8 Elemental Composition and Structural Features Structural Assembly Comments Problem 9 Elemental Composition and Structural Features Structural Assembly Comments Problem 10 Elemental Composition and Structural Features Structural Assembly Comments Problem 11 Elemental Composition and Structural Features Structural Assembly Comments Problem 12 Elemental Composition and Structural Features Structural Assembly Comments Problem 13 Elemental Composition and Structural Features Structural Assembly Comments Problem 14 Elemental Composition and Structural Features Structural Assembly Comments Problem 15 Elemental Composition and Structural Features Structural Assembly Comments Problem 16 Elemental Composition and Structural Features Structural Assembly Comments Problem 17 Elemental Composition and Structural Features Structural Assembly Comments Problem 18 Elemental Composition and Structural Features Structural Assembly Comments Problem 19 Elemental Composition and Structural Features Structural Assembly Comments Problem 20 Elemental Composition and Structural Features Structural Assembly Comments Problem 21 Elemental Composition and Structural Features Structural Assembly Comments Problem 22 Elemental Composition and Structural Features Structural Assembly Comments Problem 23 Elemental Composition and Structural Features Structural Assembly Comments Problem 24 Elemental Composition and Structural Features Structural Assembly Comments Problem 25 Elemental Composition and Structural Features Structural Assembly Comments Problem 26 Elemental Composition and Structural Features Structural Assembly Comments Problem 27 Elemental Composition and Structural Features Structural Assembly Comments Problem 28 Elemental Composition and Structural Features Structural Assembly Comments Problem 29 Elemental Composition and Structural Features Structural Assembly Comments Problem 30 Elemental Composition and Structural Features Structural AssemblyPart 3 Short Supplementing Essays Degree of Unsaturation. Calculation of Number of Double Bond Equivalents General Information from Mass Spectra Evidence for Elemental Composition from Isotope Peak Intensities Evidence for Elemental Composition in Low Resolution Mass Spectra High Resolution Data Impurities in Mass Spectra Prediction of Infrared Stretching Frequencies Overtones, Combination Bands, Fermi Resonance Band Shapes and Intensities in Infrared Spectra Spurious Bands in Infrared Spectra Rules for the Interpretation of Proton NMR Spectra General Rules Rules for First Order Spectra Higher Order Spectra Simplification of Higher Order Spectra Computer Simulation of Spectra Off-Resonance Decoupled Spectra Signal Intensities in Carbon-13 NMR Spectra Saturation Nuclear Overhauser Effect Other Influences Intensities of Solvent Signals Influence of Molecular Symmetry and Conformational Equilibria on NMR Spectra Introduction Influence of Symmetry Properties on the NMR Spectra Fast Conformational Equilibria Examples Bulk Susceptibility Corrections Solvents in Ultraviolet Spectroscopy Interactions of ChromophoresAppendix Isotope Distribution Pattern of All Natural Elements in the Periodic System Mass Correlation Table Mass Spectra of some Important Solvents which Occur Frequently as Impurity in Mass Spectra of Organic Samples Infrared Absorption Spectra of some Common Solvents and Suspension Agents Estimation of the Proton Chemical Shifts in Substituted Alkanes Estimation of the Chemical Shifts of Olefinic Protons Estimation of the Proton Chemical Shifts in Substituted Benzene Estimation of the Carbon-13 Chemical Shifts in Aliphatic Compounds Steric Corrections S Conformational Corrections C Estimation of the Chemical Shifts of Olefinic Carbon Atoms Estimation of the Carbon-13 Chemical Shifts in Substituted Benzene Estimation of the Carbon-13 Chemical Shifts in Substituted PyridineSubject IndexStructures of Compounds
- No. of pages: 288
- Language: English
- Edition: 1
- Volume: 1
- Published: December 2, 2012
- Imprint: Elsevier Science
- eBook ISBN: 9780444597540
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