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Purification of Laboratory Chemicals
Part 1 Physical Techniques, Chemical Techniques, Organic Chemicals
9th Edition - August 9, 2022
Author: W.L.F. Armarego
Paperback ISBN:9780323909679
9 7 8 - 0 - 3 2 3 - 9 0 9 6 7 - 9
eBook ISBN:9780323984430
9 7 8 - 0 - 3 2 3 - 9 8 4 4 3 - 0
Purification of Laboratory Chemicals: Part One, Physical Techniques, Chemical Techniques, Organic Chemicals, Ninth Edition describes contemporary methods for the purification of… Read more
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Purification of Laboratory Chemicals: Part One, Physical Techniques, Chemical Techniques, Organic Chemicals, Ninth Edition describes contemporary methods for the purification of chemical compounds. The work includes tabulated methods taken from literature for purifying thousands of individual commercially available chemical substances. To help in applying this information, the more common processes currently used for purification in chemical laboratories and new methods are discussed. For dealing with substances not separately listed, another chapter is included, setting out the usual methods for purifying specific classes of compounds.
Laboratory workers, whether carrying out research or routine work, will invariably need to consult this book. Apart from the procedures described, the large amount of physical data about listed chemicals is essential. This fully updated, revised and expanded new edition includes the purification of many new substances that have been available commercially since 2017, along with previously available substances which have found new applications.
Features empirical formulae and formula weights for every entry
References all important applications of each substance
Includes updated CAS registry numbers
Covers the latest commercial chemical products, including pharmaceutical chemicals and safety/hazard materials
Provides expanded coverage of laboratory/work practices and purification methods
Cover image
Title page
Table of Contents
Dedication
Copyright
Preface to the Ninth Edition
Preface to the First Edition
Preface to the Second Edition
Preface to the Third Edition
Preface to the Fourth Edition
Preface to the Fifth Edition
Preface to the Sixth Edition
Preface to the Seventh Edition
Preface to the Eighth Edition
How This Book Should Be Used
DOIs, PMIDs, ISBNs and ISSNs
Video Presentations
About the Author
Chapter 1: Common Physical Techniques Used In Purification
Abstract
Introduction
The Question Of Purity
Safety Precautions Associated With The Purification Of Laboratory Chemicals
Methods Of Purification Of Reagents And Solvents
Advances In Physical Techniques Used In Purification
Chemical And Biochemical Sources
Tables
Bibliography
Chapter 2: Chemical Methods Used in Purification
Abstract
General Remarks
Removal of Traces of Metals From Reagents
Use Of Metal Hydrides
Purification via Derivatives
General Methods for the Purification of Classes of Compounds
General Procedures for the Purification of Some Classes of Organic Compounds
Advances In Chemical Techniques Used In Purification
Bibliography
Characterisation Of Organic And Inorganic Compounds
Green Chemistry
Metal Hydrides
Spectroscopy
Trace Metal Analysis
Chapter 3: Purification of Organic Chemicals
Abstract
Introduction
3A Aliphatic Compounds
3B Alicyclic Compounds
ADDENDUM
3C Aromatic Compounds
3D Heterocyclic Compounds
General Index
CAS Registry Numbers Index
No. of pages: 662
Language: English
Published: August 9, 2022
Imprint: Butterworth-Heinemann
Paperback ISBN: 9780323909679
eBook ISBN: 9780323984430
WA
W.L.F. Armarego
Wilfred L. F. Armarego graduated BSc (Hons) in 1953 and PhD from the University of London in 1956 and came to Australia in that year. After two years at the Central Research Laboratories (ICIANZ) in Melbourne, where he worked on plant growth substances, and one year on potentially carcinogenic polycyclic aromatic hydrocarbons at the University of Melbourne as Senior Demonstrator in Organic Chemistry, he joined the Department of Medical Chemistry as a Research Fellow in 1960. He became a Fellow in 1963 and was awarded a DSc degree (London) in 1968. He was promoted to Senior Fellow in 1967 and began research work on the biochemistry and molecular biology of pteridine-requiring enzymes related to the inherited metabolic disease phenylketonuria and its variants. He was head of the Protein Biochemistry Group and Pteridine Biochemistry Laboratory until his retirement in 1996. He is now a visiting fellow at the John Curtin School of Medical Research, and member of the editorial boards of ‘Medicinal Research Reviews’ and ‘Pteridines’ journals.
Affiliations and expertise
Division of Molecular Bioscience, The John Curtin School of Medical Research, Australian National University, Canberra, Australia