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Purification of Laboratory Chemicals
7th Edition - October 17, 2012
Author: W.L.F. Armarego
Paperback ISBN:
9 7 8 - 0 - 1 2 - 3 8 2 1 6 1 - 4
eBook ISBN:
9 7 8 - 0 - 1 2 - 3 8 2 1 6 2 - 1
A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical… Read more
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A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readers on critical safety and hazards for the safe handling of chemicals and processes.The Seventh Edition is fully updated and provides expanded coverage of the latest commercially available chemical products and processing techniques, safety and hazards: over 200 pages of coverage of new commercially available chemicals since the previous edition.
- The only comprehensive chemical purification reference, a market leader since 1966, Amarego delivers essential information for research and industrial chemists, pharmacists and engineers: '... (it) will be the most commonly used reference book in any chemical or biochemical laboratory' (MDPI Journal)
- An essential lab practice and proceedures manual. Improves efficiency, results and safety by providing critical information for day-to-day lab and processing work. Improved, clear organization and new indexing delivers accurate, reliable information on processes and techniques of purification along with detailed physical properties
- The Sixth Edition has been reorganised and is fully indexed by CAS Registry Numbers; compounds are now grouped to make navigation easier; literature references for all substances and techniques have been added; ambiguous alternate names and cross references removed; new chemical products and processing techniques are covered; hazards and safety remain central to the book
Chemical Engineers, Chemists, Biochemists and Pharmaceutical Engineers who process and purify commercial chemicals in industry; university and commercial research laboratories
Dedication
Preface to the Seventh Edition
Preface to the First Edition
Preface to the Second Edition
Preface to the Third Edition
Preface to the Fourth Edition
Preface to the Fifth Edition
Preface to the Sixth Edition
How This Book Should Be Used
About the Authors
Chapter 1. Common Physical Techniques Used in Purification
Introduction
The Question of Purity
Sources of Impurities
Practices to Avoid Impurities
Safety Precautions Associated with the Purification of Laboratory Chemicals
Some Hazards of Chemical Manipulation in Purification and Recovery of Residues
Safety Disclaimer
Methods of Purification of Reagents and Solvents
Solvent Extraction and Distribution
Distillation
Recrystallisation
Sublimation
Chromatography
Electrophoresis
Drying
Properties Useful in Purification
Miscellaneous Techniques
Chemical and Biochemical Sources
Useful Websites
Bibliography
Chapter 2. Chemical Methods Used in Purification
General Remarks
Removal of Traces of Metals from Reagents
Use of Metal Hydrides
Sodium Borohydride
Purification Via Derivatives
General Methods for the Purification of Classes of Compounds
General Procedures for the Purification of Some Classes of Organic Compounds
Bibliography
Chapter 3. The Future of Purification
Introduction
Atom Economy
Organocatalysis
Microwave Technologies
Flow Chemistry
Solid Phase Synthesis
Alternative Solvents
Bibliography
Chapter 4. Purification of Organic Chemicals
Introduction
Aliphatic Compounds
Alicyclic Compounds
Aromatic Compounds
Heterocyclic Compounds
Miscellaneous as, B, P, Si, S, Se and Te Compounds
Chapter 5. Purification of Inorganic and Metal-Organic Chemicals
Introduction
Inorganic Compounds
Metal-Organic Compounds
Chapter 6. Catalysts
Introduction
Catalysts—Part 1
Organocatalysts
Catalysts—Part 2
Phase Transfer Catalysts
Tetra-n-hexylammonium chloride [5922-92-9] M 390.1. Crystallise the chloride from EtOH
Imidazolinium Ionic Liquid Crystal Catalysts
Chiral Auxiliaries
Lewis and Brønsted/Lowry Acids and Bases
Bibliography
Chapter 7. Purification of Biochemicals and Related Products
Introduction
Amino Acids and Peptides
Proteins, Enzymes, DNA and RNA
Carbohydrates
Carotenoids
Steroids
MiscelLaneous Compounds (including biologically useful reagents, low-molecular-weight bioactive substances, antibiotics, coenzymes, vitamins, lipids, phospholipids, nucleosides, nucleotides and polynucleotides)
Bibliography
Chapter 8. Nanomaterials and Nanotechnology
Introduction
Identification and Measurement of Nanomaterials
Fullerenes and Related Substances
Fullerenes
Carbon Nanotubes (CNTs) and Related Materials
Preparation of CNTs (NTs)
Purification of CNTs (NTs)
Preparation and Purification of Fullerene Pipes (TUBES)
Solubilisation of CNTs
Carbon Nanotubes (CNTs)
Functionalised CNTs
Graphene Materials
Solvent Resistant Nano Filters (SRNF)
Nano Metals and Metal Derivatives
Some Organic and Metal-Organic Compounds Used in Nanotechnology
Safety Issues
The following is a list of more recent books that were published on legal, personal, industrial, and environmental safety aspects of nanotechnology:
Bibliography
Index
CAS Registry Numbers Index
How to Validate Chemical Abstracts Service Registry Numbers
CAS Registry Numbers Index
- No. of pages: 1024
- Language: English
- Published: October 17, 2012
- Imprint: Butterworth-Heinemann
- Paperback ISBN: 9780123821614
- eBook ISBN: 9780123821621
WA
W.L.F. Armarego
Wilfred L. F. Armarego graduated BSc (Hons) in 1953 and PhD from the University of London in 1956 and came to Australia in that year. After two years at the Central Research Laboratories (ICIANZ) in Melbourne, where he worked on plant growth substances, and one year on potentially carcinogenic polycyclic aromatic hydrocarbons at the University of Melbourne as Senior Demonstrator in Organic Chemistry, he joined the Department of Medical Chemistry as a Research Fellow in 1960. He became a Fellow in 1963 and was awarded a DSc degree (London) in 1968. He was promoted to Senior Fellow in 1967 and began research work on the biochemistry and molecular biology of pteridine-requiring enzymes related to the inherited metabolic disease phenylketonuria and its variants. He was head of the Protein Biochemistry Group and Pteridine Biochemistry Laboratory until his retirement in 1996. He is now a visiting fellow at the John Curtin School of Medical Research, and member of the editorial boards of ‘Medicinal Research Reviews’ and ‘Pteridines’ journals.
Affiliations and expertise
Division of Molecular Bioscience, The John Curtin School of Medical Research, Australian National University, Canberra, Australia