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A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical re… Read more
LIMITED OFFER
Immediately download your ebook while waiting for your print delivery. No promo code needed.
A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readers on critical safety and hazards for the safe handling of chemicals and processes.The Seventh Edition is fully updated and provides expanded coverage of the latest commercially available chemical products and processing techniques, safety and hazards: over 200 pages of coverage of new commercially available chemicals since the previous edition.
Dedication
Preface to the Seventh Edition
Preface to the First Edition
Preface to the Second Edition
Preface to the Third Edition
Preface to the Fourth Edition
Preface to the Fifth Edition
Preface to the Sixth Edition
How This Book Should Be Used
About the Authors
Chapter 1. Common Physical Techniques Used in Purification
Introduction
The Question of Purity
Sources of Impurities
Practices to Avoid Impurities
Safety Precautions Associated with the Purification of Laboratory Chemicals
Some Hazards of Chemical Manipulation in Purification and Recovery of Residues
Safety Disclaimer
Methods of Purification of Reagents and Solvents
Solvent Extraction and Distribution
Distillation
Recrystallisation
Sublimation
Chromatography
Electrophoresis
Drying
Properties Useful in Purification
Miscellaneous Techniques
Chemical and Biochemical Sources
Useful Websites
Bibliography
Chapter 2. Chemical Methods Used in Purification
General Remarks
Removal of Traces of Metals from Reagents
Use of Metal Hydrides
Sodium Borohydride
Purification Via Derivatives
General Methods for the Purification of Classes of Compounds
General Procedures for the Purification of Some Classes of Organic Compounds
Bibliography
Chapter 3. The Future of Purification
Introduction
Atom Economy
Organocatalysis
Microwave Technologies
Flow Chemistry
Solid Phase Synthesis
Alternative Solvents
Bibliography
Chapter 4. Purification of Organic Chemicals
Introduction
Aliphatic Compounds
Alicyclic Compounds
Aromatic Compounds
Heterocyclic Compounds
Miscellaneous as, B, P, Si, S, Se and Te Compounds
Chapter 5. Purification of Inorganic and Metal-Organic Chemicals
Introduction
Inorganic Compounds
Metal-Organic Compounds
Chapter 6. Catalysts
Introduction
Catalysts—Part 1
Organocatalysts
Catalysts—Part 2
Phase Transfer Catalysts
Tetra-n-hexylammonium chloride [5922-92-9] M 390.1. Crystallise the chloride from EtOH
Imidazolinium Ionic Liquid Crystal Catalysts
Chiral Auxiliaries
Lewis and Brønsted/Lowry Acids and Bases
Bibliography
Chapter 7. Purification of Biochemicals and Related Products
Introduction
Amino Acids and Peptides
Proteins, Enzymes, DNA and RNA
Carbohydrates
Carotenoids
Steroids
MiscelLaneous Compounds (including biologically useful reagents, low-molecular-weight bioactive substances, antibiotics, coenzymes, vitamins, lipids, phospholipids, nucleosides, nucleotides and polynucleotides)
Bibliography
Chapter 8. Nanomaterials and Nanotechnology
Introduction
Identification and Measurement of Nanomaterials
Fullerenes and Related Substances
Fullerenes
Carbon Nanotubes (CNTs) and Related Materials
Preparation of CNTs (NTs)
Purification of CNTs (NTs)
Preparation and Purification of Fullerene Pipes (TUBES)
Solubilisation of CNTs
Carbon Nanotubes (CNTs)
Functionalised CNTs
Graphene Materials
Solvent Resistant Nano Filters (SRNF)
Nano Metals and Metal Derivatives
Some Organic and Metal-Organic Compounds Used in Nanotechnology
Safety Issues
The following is a list of more recent books that were published on legal, personal, industrial, and environmental safety aspects of nanotechnology:
Bibliography
Index
CAS Registry Numbers Index
How to Validate Chemical Abstracts Service Registry Numbers
CAS Registry Numbers Index
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