Practical Sonochemistry
Applications of Power Ultrasound in Chemistry and Processing
- 3rd Edition - January 31, 2025
- Authors: Timothy J Mason, Mircea Vinatoru
- Language: English
- Paperback ISBN:9 7 8 - 0 - 4 4 3 - 2 2 0 5 4 - 8
- eBook ISBN:9 7 8 - 0 - 4 4 3 - 2 2 0 5 3 - 1
Practical Sonochemistry: Applications of Power Ultrasound in Chemistry and Processing, Third Edition conveys the increasing growth in applications and equipment to power ultrasoun… Read more
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Request a sales quotePractical Sonochemistry: Applications of Power Ultrasound in Chemistry and Processing, Third Edition conveys the increasing growth in applications and equipment to power ultrasound. The book is written primarily for graduate students, postdoc researchers, and academics in applied chemistry and chemical engineering, as well as technicians and operators in relevant industry. Sonochemistry can do lots of amazing things in many different fields – but how and where do you start with applying it? This thoroughly updated edition offers a ground-up introduction to the fundamentals, applying power ultrasound to both lab and large-scale applications.
The book answer questions such as:
- Does my laboratory have the equipment- what do I need?
- I have the equipment, but I have no idea how it works or how to use it- where do I start?
- I want to apply sonochemistry to a new reaction or processing method – what is the best approach?
- What types of sonochemistry equipment are available on the market and which is the best to choose?
- Can I scale up my reaction and if so, how do I do it, given that ultrasound is non-linear?
- Fully updated third edition conveys the increasing growth in applications and equipment to power ultrasound
- Provides detailed descriptions of the newest ultrasonic equipment and its applications, which offer a wide range of frequencies with more reproducible experimentation and a variety of scale-up systems
- Demonstrates the practical laboratory uses of ultrasound technology for industrial scale performance
- Includes useful exercises to familiarize readers with sonochemical operations
Written primarily for graduate students, postdoc researchers and academics in the fields of applied chemistry and chemical engineering who want to make use of sonochemistry in their work, as well as practitioners working in industries with the relevant processing technologies who are using power ultrasound. This book may also be utilized by graduate students, postdoc researchers, academics, and industry professionals in adjacent fields such as environmental science, extraction of vegetal constituents, food technology and materials science who may also wish to use power ultrasound
1. Introduction to the Uses of power ultrasound in chemistry
1.1 A brief history of power ultrasound and sonochemistry
1.2 Some comments on the general effects of ultrasound
1.3 Cavitation—the origin of sonochemical effects
1.4 The physical, chemical, and biological effects of acoustic cavitation
1.5 The generation of ultrasound—transducers
1.6 The coupling of ultrasound to liquids
1.7 Types of sonochemistry equipment
1.8 Dosimetry for ultrasonic systems
1.9 Some comments on the mechanical effects of ultrasound
1.10 The effects of frequency on sonochemistry
1.11 The sonochemical yield
1.12 The safety of sonochemical equipment
2. The ultrasonic cleaning bath or tank
2.1 Bath design and construction
2.2 Choosing the correct type of ultrasonic bath
2.3 Setting up an ultrasonic bath for sonochemistry
2.4 Advantages and disadvantages of using an ultrasonic bath for
sonochemistry
3. The ultrasonic probe
3.1 The components of an ultrasonic probe system
3.2 Choosing a probe system for sonochemistry
3.3 Laboratory reactors involving probe systems
3.4 Advantages and disadvantages of using an ultrasonic probe system for
sonochemistry
4. Hydrodynamic cavitation reactors
4.1 Hydrodynamic cavitation reactors
4.2 History of hydrodynamic cavitation
4.3 Methods of generating hydrodynamic cavitation
4.4 Comparison of acoustic and hydrodynamic cavitation
4.5 Some applications of hydrodynamic cavitation
4.6 Conclusions
5. Large-scale sonochemistry
5.1 Challenges involved in the scale up of sonochemistry
5.2 Large-scale systems using ultrasonic tanks
5.3 Large-scale systems using ultrasonic probes
5.4 Tubular reactors with resonating walls
5.5 Other large-scale ultrasonic processors
5.6 Future prospects
6. Practical laboratory demonstrations of sonochemistry
6.1 Laboratory demonstrations of the effects of sonochemistry
6.2 Laboratory experiments illustrating various aspects of sonochemistry
1.1 A brief history of power ultrasound and sonochemistry
1.2 Some comments on the general effects of ultrasound
1.3 Cavitation—the origin of sonochemical effects
1.4 The physical, chemical, and biological effects of acoustic cavitation
1.5 The generation of ultrasound—transducers
1.6 The coupling of ultrasound to liquids
1.7 Types of sonochemistry equipment
1.8 Dosimetry for ultrasonic systems
1.9 Some comments on the mechanical effects of ultrasound
1.10 The effects of frequency on sonochemistry
1.11 The sonochemical yield
1.12 The safety of sonochemical equipment
2. The ultrasonic cleaning bath or tank
2.1 Bath design and construction
2.2 Choosing the correct type of ultrasonic bath
2.3 Setting up an ultrasonic bath for sonochemistry
2.4 Advantages and disadvantages of using an ultrasonic bath for
sonochemistry
3. The ultrasonic probe
3.1 The components of an ultrasonic probe system
3.2 Choosing a probe system for sonochemistry
3.3 Laboratory reactors involving probe systems
3.4 Advantages and disadvantages of using an ultrasonic probe system for
sonochemistry
4. Hydrodynamic cavitation reactors
4.1 Hydrodynamic cavitation reactors
4.2 History of hydrodynamic cavitation
4.3 Methods of generating hydrodynamic cavitation
4.4 Comparison of acoustic and hydrodynamic cavitation
4.5 Some applications of hydrodynamic cavitation
4.6 Conclusions
5. Large-scale sonochemistry
5.1 Challenges involved in the scale up of sonochemistry
5.2 Large-scale systems using ultrasonic tanks
5.3 Large-scale systems using ultrasonic probes
5.4 Tubular reactors with resonating walls
5.5 Other large-scale ultrasonic processors
5.6 Future prospects
6. Practical laboratory demonstrations of sonochemistry
6.1 Laboratory demonstrations of the effects of sonochemistry
6.2 Laboratory experiments illustrating various aspects of sonochemistry
- No. of pages: 256
- Language: English
- Edition: 3
- Published: January 31, 2025
- Imprint: Elsevier Science
- Paperback ISBN: 9780443220548
- eBook ISBN: 9780443220531
TJ
Timothy J Mason
Tim Mason is Emeritus Professor of Chemistry and Director of the Sonochemistry Centre at the University of Coventry, UK. He graduated from Southampton University, UK in 1967 with a BSc in Chemistry and continued his career in the research field of physical organic chemistry with a PhD from the same university and two years as a post-doc at Amherst College in Massachusetts, USA. He began research into sonochemistry at Coventry University with his first paper on the subject published in 1980. He became the first president of the European Society of Sonochemistry when it was formed in 1991 until 2014 and became editor of Ultrasonics Sonochemistry from its first issue in 1994 until he retired as Editor in Chief in 2017. He has authored and edited 11 textbooks and the six-volume series “Advances in Sonochemistry”. Since his retirement and appointment as emeritus professor at Coventry University, he has continued his research interests in a broad range of topics which include fundamental aspects of sonochemistry, reactor design and scale-up, environmental protection, food processing, ultrasonically assisted extraction (UAE), materials processing and therapeutic ultrasound. Currently his main research collaboration is with co-author Mircea Vinatoru through the ULTRA-MINT programme.
Affiliations and expertise
Professor Emeritus of Chemistry and Director, the Sonochemistry Centre, University of Coventry, UKMV
Mircea Vinatoru
Mircea Vinatoru is a principal investigator at Politehnica University of Bucharest, Romania where he directed a European/Romanian research programme involving the use of hybrid ultrasound and microwave technologies in a range of chemical reactions (ULTRA-MINT). He has over 50 years of experience in organic chemistry research of which the last 32 were dedicated to sonochemistry. During his career in sonochemistry he studied electron transfer processes facilitated by ultrasound as part of his PhD thesis. He was a pioneer in two major fields – the ultrasonically assisted synthesis of biodiesel fuel (UASB) and ultrasonically assisted extraction (UAE) of bioactive compounds from medicinal and aromatic herbs, in both of which he holds patents. In the medical field he has published papers on the use of ultrasound to produce self-sterilizing fabrics and the synthesis of targeted drug delivery systems. Other contributions have been on the applications of ultrasound in environmental protection and its use in enzyme activation. He is a chemical engineer and has designed and built the first industrial reactor for ultrasonically assisted extraction of medicinal herbs and pilot scale reactors for biodiesel synthesis. He holds many research positions in public research institutes and universities in Romania and abroad. He has also assembled a sonochemistry research facility in Texas, USA where new technologies for biodiesel synthesis assisted by ultrasound were developed. He has more than 80 publications which have received over 6000 citations.
Affiliations and expertise
Principal Investigator, Faculty of Chemical Engineering and Biotechnology, University Politehnica of Bucharest, Romania