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Introductory Titrimetric and Gravimetric Analysis
The Commonwealth and International Library: Chemistry Division
- 1st Edition - January 1, 1966
- Author: Evelyn M. Rattenbury
- Language: English
- Hardback ISBN:9 7 8 - 0 - 0 8 - 0 1 1 9 5 0 - 2
- Paperback ISBN:9 7 8 - 1 - 4 8 3 1 - 2 4 5 2 - 0
- eBook ISBN:9 7 8 - 1 - 4 8 3 1 - 5 6 9 4 - 1
Introductory Titrimetric and Gravimetric Analysis is an introductory course to the general principles of titrimetric and gravimetric analysis of chemical solutions and substances.… Read more
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Request a sales quoteIntroductory Titrimetric and Gravimetric Analysis is an introductory course to the general principles of titrimetric and gravimetric analysis of chemical solutions and substances. The book is divided in two parts. Part I focuses on the principles of titrimetric analysis, covering topics on acid-base, argentometric, oxidation-reduction, iodometric, and complexometric titrations. Part II covers the principles of gravimetric analysis, discussing gravimetric process and methods; and the gravimetric determinations of several chemical solutions and substances. Chemists and students of chemistry will find the book a good reference material.
Part 1. Titrimetric Analysis
1. Introduction and General Principles
The Preparation of a Standard Solution
The Titration of Weighed Quantities of Substances
Titrations
The Indicator
Method of Titration Using Two Burettes
Primary Standard Substances
Accuracy in Titrimetric Analysis
Calibration of Titrimetric Apparatus
The Laboratory Practical Notebook
Cleanliness and Care of the Burette and Pipette
2. Acid-Base Titrations
Choice of Indicator for a Particular Titration
Table of Some Indicators
Determination of the Concentration of a Solution of Sodium Hydroxide, Given Oxalic Acid Crystals, with Subsequent Determination of the Concentration of a Solution of Hydrochloric Acid
Writing-up of Titrimetric Determinations
Standardization of a Solution of Sulphuric Acid Using Borax and Subsequent Checking of the Result Using Anhydrous Sodium Carbonate
Acidic Primary Standards
Determinations Using Standard Acid or Standard Alkali Solutions
Suggestions for Variations on Acid-base Titration Exercises
3. Argentometric Titrations
Standardization of Silver Nitrate Solution, Given Sodium Chloride Crystals
A Method for the Recovery of Silver Nitrate from "Residues"
Determinations Using Standardized Silver Nitrate Solutions
Suggestions for Variations on Silver Nitrate Titration Exercises
4. Oxidation-Reduction Titrations
Standardization of a Potassium Permanganate Solution Using Ammonium Ferrous Sulphate and Checking the Result with Sodium Oxalate
Determinations Using Standardized Potassium Permanganate Solutions
Suggestions for Variations in Potassium Permanganate and Potassium Dichromate Titration Exercises
5. Iodometric Titrations
Standardization of a Sodium Thiosulphate Solution, Using Potassium Iodate and Checking the Result with Potassium Dichromate
Determinations Using Standardized Sodium Thiosulphate Solutions
Suggestions for Variations in Iodometric Titration Exercises
6. Complexometric Titrations
Determinations Using Standard Ethylenediamine-tetra-acetic Acid Solutions
Suggestions for Variations on Ethylenediamine-tetra-acetic Acid Titration Exercises
Part II. Gravimetric Analysis
7. Introduction and General Principles
The Physical Properties of the Precipitate
Contamination of Precipitates
Precipitation from Homogenous Solution
Washing Precipitates
Drying of a Precipitate
Apparatus
Recording of Results
Accuracy
8. Selected Gravimetric Determinations
Determination of Water of Crystallization
Determination of Iron in Ammonium Iron Alum
Determination of Lead as Lead Chromate
Determination of Nickel as Nickel Dimethylglyoxime Complex
Determination of Aluminum as Aluminum 8-hydroxyquinolate
Determination of Chloride as Silver Chloride
Determination of Sulphate as Barium Sulphate
Suggestions for Variations on the Described Gravimetric Exercises
Bibliography
Tables
Some Atomic Weights
Some Primary Standard Substances
Some Concentrated Reagents
Logarithms
Antilogarithms
Index
- No. of pages: 200
- Language: English
- Edition: 1
- Published: January 1, 1966
- Imprint: Pergamon
- Hardback ISBN: 9780080119502
- Paperback ISBN: 9781483124520
- eBook ISBN: 9781483156941
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