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Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the… Read more
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PREFACE
Chapter 1: GENERAL INTRODUCTION
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The Nature of Organic Reactions
Basic Principles of Preparative Organic Chemistry
Unit Operations
Reports and Communications
Good Laboratory Practice
Yields and Losses—Their Calculation and Importance
Chapter 2: REVIEW OF APPARATUS AND EQUIPMENT
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Glassware
Ground-glass Fittings
Corks and Bungs
Size of Apparatus
Cleaning and Drying Glassware
Chapter 3: HAZARDS
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Toxicity
Bodily Injuries
Smoking
Fire
Explosion
Implosion
General Attitude to Hazards
Chapter 4: TECHNIQUES AND UNIT OPERATIONS FOR CARRYING OUT A REACTION
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General Principles
Materials Handling
Assembly of Apparatus
Heat Transfer
Chapter 5: TECHNIQUES AND UNIT OPERATIONS FOR ISOLATING AND PURIFYING A REACTION PRODUCT
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Distillation
Extraction
Recrystallization
Precipitation
Filtration
Chapter 6: DRYING
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Drying Solids
Drying Liquids
Drying Gases
Chapter 7: CRITERIA OF PURITY
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Determination of a Melting Point
Mixed Melting Points: Identifying a Compound
Refractive Index
Chromatography
Chapter 8: PACKING AND STORING PRODUCTS AND SAMPLES
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Solids
Liquids
Labels for Samples, etc
Chapter 9: REPORTS AND COMMUNICATIONS
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APPENDIX: SPECIMEN LABORATORY NOTEBOOK RECORDS
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