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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has ga… Read more
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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.
Contributors
Preface
Chapter One. NMR Studies of Crown Ether–Cyclodextrin Complexes
Abstract
1 Introduction
2 Cyclodextrins: The Molecular Containers
3 Crown Ethers and Cryptands: The Beginning of Supramolecular Chemistry
4 Cyclodextrin–Crown Ether Complexes: Non-NMR Studies
5 Cyclodextrin–Crown Ether Interactions: An NMR Look
6 Complexes of Cyclam Derivatives
7 Conclusions
References
Chapter Two. 15N and 31P NMR Coordination Shifts in Transition Metal Complexes with Nitrogen- and Phosphorus-Containing Heterocycles
Abstract
1 Transition Metal Complexes with Azines
2 Transition Metal Complexes with Azoles
3 Transition Metal Complexes with Purines
4 Transition Metal Complexes with 1,2,4-Triazolo-[1,5a]-Pyrimidines
5 Transition Metal Complexes with Phosphinines
6 Transition Metal Complexes with Phospholes
7 Conclusions
References
Chapter Three. Quantification of Complex Mixtures by NMR
Abstract
1 Introduction
2 Practical Background
3 NMR Acquisition Methods
4 Post-Acquisition NMR Processing
5 Application Areas of qNMR
6 Future Developments
Acknowledgements
References
Chapter Four. Proton NMR Profiling of Food Samples
Abstract
1 Introduction
2 Sample Preparation
3 NMR Techniques
4 Data Treatment
5 Statistical Analysis
6 Applications
References
Chapter Five. Magic Angle Spinning NMR Studies of Protein Assemblies: Recent Advances in Methodology and Applications
Abstract
1 Introduction
2 Recent Methodological Advances for MAS NMR Studies of Protein Assemblies
3 Recent MAS NMR Applications to Study Protein Assemblies
4 Conclusions and Outlook
References
Chapter Six. Recent Advances in Solution NMR Studies: 13C Direct Detection for Biomolecular NMR Applications
Abstract
1 Introduction
2 Intrinsic Properties of Heteronuclei (13C, 15N)
3 Examples of Applications
References
Index
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