An Approach to Chemical Analysis
Its Development and Practice
- 1st Edition - November 11, 2013
- Latest edition
- Author: H. N. Wilson
- Editors: Robert Robinson, L. A. K. Staveley, H. M. N. H. Irving
- Language: English
- Paperback ISBN:9 7 8 - 1 - 4 8 3 1 - 6 9 9 2 - 7
- eBook ISBN:9 7 8 - 1 - 4 8 3 1 - 8 5 7 3 - 6
An Approach to Chemical Analysis: Its Development and Practice provides an overview of the development of chemical analysis and its application in solving analytical problems in… Read more
An Approach to Chemical Analysis: Its Development and Practice provides an overview of the development of chemical analysis and its application in solving analytical problems in chemistry. The text is comprised of 19 chapters that are organized into two parts. In the first part, the text covers the historical aspects of chemical. The book then proceeds to tackling methods for analysis in which the final measurement is preceded by one or more chemical reactions. The first two chapters of the second part discuss distillation and chromatography, respectively. Next, the title details the physical methods that only occasionally and incidentally need to be preceded by chemical reactions. The text will be of great use for students, researchers, and practitioners of chemistry.
AUTHOR’S PREFACE
PART I
CHAPTER 1: THE EARLY HISTORY OF CHEMICAL ANALYSIS
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CHAPTER 2: "CLASSICAL" ANALYSIS AND THE IMPACT OF PHYSICAL CHEMISTRY
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THE ROLE OF PHYSICAL CHEMISTRY—FROM 1870 ONWARDS
PHYSICAL CHEMISTRY AND COMPLEX IONS
PHYSICAL CHEMISTRY AND THE PHENOMENA OF PRECIPITATION
CHAPTER 3: THE FIRST ORGANIC REAGENTS
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α-NITROSO-β-NAPHTHOL
DIMETHYLGLYOXIME
CUPFERRON
CHAPTER 4: ORGANIC ANALYSIS
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GENERAL ORGANIC ANALYSIS
ORGANIC ANALYSIS IN IMPORTANT INDUSTRIES
CHAPTER 5: LARGE-SCALE INDUSTRY AND VOLUMETRIC ANALYSIS
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THE GROWTH OF VOLUMETRIC ANALYSIS
CHAPTER 6: THE MODERN APPROACH TO CHEMICAL ANALYSIS
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LATER DEVELOPMENTS IN INORGANIC CHEMICAL ANALYSIS
SPECTROPHOTOMETRY OF DITHIZONE SOLUTIONS
pH VALUE AND THE APPARENT CO-EFFICIENT OF EXTRACTION
EXAMPLES OF THE USE OF DITHIZONE
OTHER NEW REAGENTS
CHAPTER 7: ORGANIC MICRO-ANALYSIS
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QUANTITATIVE MICRO-ANALYSIS
DETERMINATION OF OXYGEN
FURTHER ADVANCES IN MICRO-ANALYSIS
CHAPTER 8: USE OF NON-AQUEOUS SOLVENTS IN ANALYSIS
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1 AS TITRATION MEDIUM
2 USE OF NON-AQUEOUS SOLVENTS FOR THE EXTRACTION OF METALS
CHAPTER 9: POLAROGRAPHY
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THE BASE SOLUTION
THE NATURE OF THE ANODE
USES OF POLAROGRAPHY
RECENT DEVELOPMENTS OF POLAROGRAPHY
THE CATHODE RAY POLAROGRAPH
CHAPTER 10: OTHER ELECTROCHEMICAL METHODS
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ELECTRODEPOSITION
COULOMETRY
POTENTIOMETRY
AMPEROMETRIC TITRATION
THE POLARIZATION END-POINT; THE “DEAD STOP END-POINT”
CONDUCTIMETRIC TITRATION AND HIGH FREQUENCY TITRATION
HIGH FREQUENCY TITRATION
PART II: INTRODUCTION
INTRODUCTION TO INTRODUCTION
USES OF THE PRINCIPAL PHYSICAL METHODS OF ANALYSIS
CHAPTER 11: FRACTIONAL DISTILLATION
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THE CONCEPT OF THE “THEORETICAL PLATE” AND ITS PRACTICAL REALIZATION
CHAPTER 12: CHROMATOGRAPHY
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LIQUID-SOLID CHROMATOGRAPHY
PARTITION LIQUID-LIQUID CHROMATOGRAPHY
GAS CHROMATOGRAPHY
CHAPTER 13: ABSORPTIOMETRY AND "COLORIMETRIC ANALYSIS"
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INTRODUCTION
VALIDITY OF LAMBERT-BEER LAWS
ACCURACY OF ABSORPTIOMETRY
INSTRUMENTATION
ULTRA-VIOLET ANALYSIS
USES OF ULTRA-VIOLET SPECTROPHOTOMETRY
NON-DISPERSIVE INFRA-RED GAS ANALYSIS
FLUORIMETRIC ANALYSIS
CHAPTER 14: EMISSION SPECTROSCOPY
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APPARATUS FOR SPECTROGRAPHY
PREPARATION AND ANALYSIS OF SAMPLES
METAL ANALYSIS
INTERPRETATION OF THE SPECTRA OBTAINED
FLAME PHOTOMETRY
CHAPTER 15: ATOMIC ABSORPTION SPECTROPHOTOMETRY
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CHAPTER 16: APPLICATIONS OF X-RAYS TO CHEMICAL ANALYSIS
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1 X-RAY ANALYSIS BY ABSORPTION
2 X-RAY ANALYSIS BY CRYSTAL DIFFRACTION
3 X-RAY FLUORESCENCE ANALYSIS
CHAPTER 17: APPLICATIONS OF RADIOACTIVITY TO CHEMICAL ANALYSIS
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THE NATURE OF RADIOACTIVITY
METHODS OF MEASURING RADIOACTIVITY
INSTRUMENTS USED
THE METHODS OF RADIOACTIVE ANALYSIS
PRINCIPLES OF NEUTRON ACTIVATION ANALYSIS
THE COURSE OF THE ANALYSIS
SUGGESTIONS FOR READING
CHAPTER 18: MASS SPECTROMETRY
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THE MASS SPECTROMETER
OPERATION
CHAPTER 19: CHEMICAL ANALYSIS; ART, CRAFT, OR SCIENCE?
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INDEX
- Edition: 1
- Latest edition
- Published: November 11, 2013
- Language: English
RR
Robert Robinson
Affiliations and expertise
Recently retired from editorship of Canadian Security magazineRead An Approach to Chemical Analysis on ScienceDirect