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Thermal Analysis
From Introductory Fundamentals to Advanced Applications
1st Edition - June 23, 2021
Authors: El-Zeiny Ebeid, Mohamed Barakat Zakaria
Paperback ISBN:
9 7 8 - 0 - 3 2 3 - 9 0 1 9 1 - 8
eBook ISBN:
9 7 8 - 0 - 3 2 3 - 9 0 1 9 2 - 5
Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth… Read more
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Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry.
Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management.
- Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding
- Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs
- Contains chapters that cover the user of TA in materials science and crystal structures
Researchers using Thermal Analysis in materials design, chemical engineering, food quality, chemicals, electronics, industrial chemistry, and waste management and recycling. Upper undergraduate and graduate students and educators in chemistry, physics, physical science, and materials science
Chapter I: State-of-the-Art and Definitions of Various Thermal Analysis Techniques
DefinitionsInstrumentation of DSC and DTADifferential photo-calorimetry (DPC)Pressure differential scanning calorimetry (PDSC)Low temperature type DSCGeneral thermodynamic relationshipsThermogravimetry (TG) or thermogravimetric analysis (TGA)Thermomechanical analysis (TMA)Dynamic mechanical analysis (DMA)Dielectric thermal analysis (DEA)Thermally- stimulated current (TSC)Emanation thermal analysis (ETA)Thermoluminescence (TL)Fast scanning calorimetry (FSC)MicrocalorimetryLaser flash method thermal constant measuring LF/TCMMoisture evolution analyzers (MEA)Thermal analysis data processing systemSummaryReferenceChapter 2: Temperature-Modulated DSC (TMDSC)Production of nanostructured metal oxidesEstimation of carbon contentProduction of metal carbides and metals and alloys nanoparticlesProduction of metal sulfides, selenides and phosphidesTGA in sol-gel scienceEstimation of metal’s molar massEstimating oxygen content in metal oxidesCarbonizationSummaryReferences
Chapter 3: Thermal Analysis in Materials ScienceProduction of nanostructured metal oxidesEstimation of carbon contentProduction of metal carbides and metals and alloys nanoparticlesProduction of metal sulfides, selenides and phosphidesTGA in sol-gel scienceEstimation of metal’s molar massEstimating oxygen content in metal oxidesCarbonizationSummaryReferences
Chapter 4: Applications of TATA in food industryTA of soap and detergentsTA in electronics industryPolymer crystallinityPolymer blendsTA in fossil fuel researchTA in claysTA in cement industryTA in explosivesTA in testing the loading efficiencies of drugsTA in solid state reaction kineticsSummaryReferences
Chapter 5: Thermal Analysis in Studying the Phase ProblemCrystal structure transformationTopotactic thermal conversionConstructing phase diagrams using TA techniquesThermoelectric materialsPhase transformations in organic compounds and drugsSummaryReferences
Chapter 6: Thermal Analysis in Recycling and Waste ManagementIdentity of the mixed recycled plastics using DSCTGA in the transformation processes of waste rubber and plastic products for energy carriersTGA characteristics and kinetics of scrap tyre- biomass co-pyrolysisCapture of organic iodides from nuclear wasteChalcogenide aerogels as sorbents for radioactive iodineSandia Octahedral Molecular Sieves (SOMS) and their related perovskites in nuclear waste managementStudy of nuclear graphite using TGAThermal oxidation of nuclear graphiteThermal characteristics of spent activated carbon (SAC) generated from air cleaning unitsCold-cap reactions in vitrification of nuclear waste glassTA in vitrification of radioactive spent ion exchange resins (SIER) in borosilicate glassTA in electronics waste recyclingSummaryReferences
- No. of pages: 320
- Language: English
- Published: June 23, 2021
- Imprint: Elsevier
- Paperback ISBN: 9780323901918
- eBook ISBN: 9780323901925
EE
El-Zeiny Ebeid
El-Zeiny M. Ebeid is a Professor of Physical Chemistry, Tanta University, Egypt. He received his PhD under joint supervision between Tanta University and UCW, UK in 1980. He was a Visitor to the University of Kent at Canterbury and Kon-stanz Universities. He won the Egyptian National Academy of Science Award. He co-authored several published books including the book Photophysical and Laser-Based Techniques in Chemistry, Biology and Medicine, Book Surge Publisher (2006), USA. He is a Member of the American Nano Society. He has more than 80 publications in international scientific Journals. His areas of interest are in the fields of laser chemistry, solid state chemistry, and nanomaterials.
Affiliations and expertise
Professor, Physical Chemistry, Department of Chemistry, Faculty of Science, Tanta University, EgyptMZ
Mohamed Barakat Zakaria
Mohamed B. Zakaria is a Lecturer of Physical Chemistry, Tanta University, Egypt. He received his BSc in Chemistry and MSc in Physical Chemistry from Tanta University and his PhD (2016) in Engineering from Waseda University, Tokyo, Japan. He did his postdoctoral research at National Institute for Materials Science as a JSPS Fellow from 2016-2018. He is a research Fellow of National Institute for Materials Science, Tsukuba, Japan; and Australian Institute for Bioengineering and Nanotechnology (AIBN), The University of Queensland (UQ), Brisbane, Australia. Mohamed was awarded a Humboldt Research Fellowship in March 2020 at Ruhr University Bochum and Fraunhofer UMSICHT, Bochum, Germany. He’s received many awards including IAAM Young Scientist Prestigious Medal (2018) and IAAM Lecture Award (2020), best posters award of Energy & Environmental Science and APL Materials journals (2015). He has published 50 articles in the fields of Nanostructured Materials Engineering for Energy Storage and Conversion, Catalysis & Electronics
Affiliations and expertise
Lecturer, Physical Chemistry and Researcher, International Research Center for Materials Nanoarchitechtonics (MANA), National Institute for Materials Science (NIMS), Tsukuba, Japan