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Synthesis of Nanostructured Materials in Near and/or Supercritical Fluids
Methods, Fundamentals and Modeling
- 1st Edition, Volume 8 - November 27, 2021
- Authors: Can Erkey, Michael Turk
- Language: English
- Paperback ISBN:9 7 8 - 0 - 4 4 4 - 6 4 0 8 9 - 5
- eBook ISBN:9 7 8 - 0 - 4 4 4 - 6 4 0 9 0 - 1
Synthesis of Nanostructured Materials in Near and/or Supercritical Fluids: Methods, Fundamentals and Modeling offers a comprehensive review of the current status of research,… Read more
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Request a sales quoteSynthesis of Nanostructured Materials in Near and/or Supercritical Fluids: Methods, Fundamentals and Modeling offers a comprehensive review of the current status of research, development and insights on promising future directions, covering the synthesis of nanostructured materials using supercritical fluid-based processes. The book presents fundamental aspects such as high-pressure phase behavior of complex mixtures, thermodynamics and kinetics of adsorption from supercritical solutions, mechanisms of particle formation phenomena in supercritical fluid-based processes, and models for further development. It bridges the gap between theory and application, and is a valuable resource for scientists, researchers and students alike.
- Includes thermodynamic and mass transfer data necessary for industrial plant design
- Explains the mechanisms of reactions in a supercritical fluid environment
- Lists numerous industrial processes for the production of many consumer products
Chemical engineers, materials scientists, chemists and physicists from both, academia and industry. The book could be used for a graduate level course on supercritical fluids
- Cover image
- Title page
- Table of Contents
- Copyright
- Foreword
- Preface
- Chapter 1: Introduction
- Abstract
- 1.1: Some conventions
- 1.2: Motivation
- 1.3: Scope of the book
- References
- Chapter 2: Compounds of interest
- Abstract
- 2.1: Introduction
- 2.2: Types of coordination compounds
- 2.3: Structures and bonding in coordination compounds
- 2.4: Reactions of organometallic compounds on surfaces
- Chapter 3: Support materials
- Abstract
- 3.1: Different support materials
- 3.2: Characterization of porous materials
- References
- Chapter 4: Fundamental aspects of pure supercritical fluids
- Abstract
- 4.1: Introduction
- 4.2: Thermal and caloric properties
- 4.3: Transport properties
- 4.4: Applications of supercritical fluids
- References
- Chapter 5: Thermodynamics and transport properties of mixtures composed of metal complexes and supercritical fluids
- Abstract
- 5.1: Introduction
- 5.2: Phase behavior
- 5.3: Solubility and binary diffusion coefficients of metal complexes in SCF
- 5.4: Determination of high-pressure phase behavior data
- 5.5: Experimental procedure
- 5.6: Modeling solubility of metal complexes in SCFs
- 5.7: Experimental determination and modeling of the solubility of salts in sub and supercritical H2O
- References
- Chapter 6: Thermodynamics and kinetics of adsorption of metal complexes on surfaces from supercritical solutions
- Abstract
- 6.1: Adsorption
- 6.2: Adsorption isotherms
- 6.3: Adsorption of supercritical fluids
- 6.4: Adsorption of solutes from supercritical mixtures
- 6.5: Adsorption of metal complexes on surfaces
- References
- Chapter 7: Synthesis of nanostructured composites of metals by supercritical deposition (SCD)
- Abstract
- 7.1: Supported nanoparticles on inorganic and carbon supports
- 7.2: Polymer supported nanoparticles
- 7.3: Supported bimetallic and multimetallic nanoparticles
- 7.4: Metallic films
- 7.5: Comparison with other methods
- References
- Chapter 8: Synthesis of metal oxide nanoparticles
- Abstract
- 8.1: Introduction
- 8.2: Basics of continuous hydrothermal synthesis (CHTS) in sub/supercritical water
- 8.3: Experimental procedure
- 8.4: Summary and outlook
- References
- Chapter 9: Modeling of particle formation in supercritical fluids (SCF)
- Abstract
- 9.1: Introduction
- 9.2: SFRD process
- 9.3: CHTS process
- 9.4: Supplementary explanations on the application of the general dynamic equation
- References
- Chapter 10: Future research needs and developments
- Abstract
- 10.1: Synthesis of mono and bimetallic nanoparticles
- 10.2: Synthesis of metal oxide nanoparticles
- Index
- No. of pages: 282
- Language: English
- Edition: 1
- Volume: 8
- Published: November 27, 2021
- Imprint: Elsevier
- Paperback ISBN: 9780444640895
- eBook ISBN: 9780444640901
CE
Can Erkey
Can Erkey works in the Department of Chemical and Biological Engineering at Koc University in Istanbul, Turkey.
Affiliations and expertise
Department of Chemical and Biological Engineering, Koc University, Istanbul, TurkeyMT
Michael Turk
Michael Türk received his Dipl.-Ing. degree in Chemical Engineering from the Universität Karlsruhe (Technische Hochschule). In 1993 M. Türk completed his PhD thesis in the field of thermodynamic properties and intermolecular interactions of binary gaseous mixtures. In his professorial dissertation of 2001 a theory was proposed allowing understanding of the relationship between process conditions and the properties of organic particles produced by supercritical fluid based processes.
His current research activities are focused on the use of supercritical fluids (mainly CO2 and H2O) as media to prepare organic, inorganic and metallic materials by physical transformation or chemical reaction and the development of new, energy-efficient and environmentally-friendly strategies to create novel products with extraordinary performance for pharmaceutical, energy and biomedical applications.
So far, M. Türk has authored 125 articles (including 13 book chapters); has graduated 20 PhD students (10 as supervisor and 10 as co-advisor) and more than 50 Diploma / Master and 15 Bachelor students.
Affiliations and expertise
Institute for Technical Thermodynamics and Refrigeration, Karlsruhe Institute of Technology (KIT), Baden-Wuerttemberg, GermanyRead Synthesis of Nanostructured Materials in Near and/or Supercritical Fluids on ScienceDirect