Solution Methods for Metal Oxide Nanostructures

1st Edition - June 27, 2023
Imprint: Elsevier
Editors: Rajaram S. Mane, Vijaykumar Jadhav, Abdullah M. Al-Enizi
Language: English
Paperback ISBN:
9 7 8 - 0 - 1 2 - 8 2 4 3 5 3 - 4
eBook ISBN:
9 7 8 - 0 - 3 2 3 - 8 5 3 3 2 - 3

Solution Methods for Metal Oxide Nanostructures reviews solution processes that are used for synthesizing 1D, 2D and 3D metal oxide nanostructures in either thin film or in powder… Read more

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Solution Methods for Metal Oxide Nanostructures reviews solution processes that are used for synthesizing 1D, 2D and 3D metal oxide nanostructures in either thin film or in powder form for various applications. Wet-chemical synthesis methods deal with chemical reactions in the solution phase using precursors at proper experimental conditions. Wet-chemical synthesis routes offer a high degree of controllability and reproducibility for 2D nanomaterial fabrication. Solvothermal synthesis, template synthesis, self-assembly, oriented attachment, hot-injection, and interface-mediated synthesis are the main wet-chemical synthesis routes for 2D nanomaterials. Solution Methods for Metal Oxide Nanostructures also addresses the thin film deposition metal oxides nanostructures, which plays a very important role in many areas of chemistry, physics and materials science.

Each chapter includes information on a key solution method and their application in the design of metal oxide nanostructured materials with optimized properties for important applications. The pros and cons of the solution method and their significance and future scope is also discussed in each chapter. Readers are provided with the fundamental understanding of the key concepts of solution synthesis methods for fabricating materials and the information needed to help them select the appropriate method for the desired application.

Cover Image
The Metal Oxides Book Series Edited by Ghenadii Korotcenkov
Title Page
Copyright
Table of Contents
Contributors
Series editor biography
Preface
Part I Introduction
Chapter 1 Introduction to wet chemical methods and metal oxide nanostructures
1.1 Introduction
1.2 Sol-Gel
1.3 Hydrothermal
1.4 Electrochemical deposition
1.5 Chemical bath deposition
1.6 Successive ion layer adsorption and reaction deposition
1.7 Conclusions
References
Part II Synthesis of metal oxide nanostructures
Chapter 2 Sol-gel technology for the synthesis of metal oxide nanostructures
2.1 Introduction
2.2 Essential components and experimental design
2.3 Synthesis of metal oxide nanostructures
2.4 Conclusions and future perspectives
References
Chapter 3 Co-precipitation methods for the synthesis of metal oxide nanostructures
3.1 Introduction
3.2 Growth mechanism
3.3 Synthesis of metal oxides
3.4 Other oxide materials
3.5 Conclusions
References
Chapter 4 Microwave mediated chemical synthesis of metal oxide nanostructures for electrochemical supercapacitors
4.1 Introduction
4.2 Microwave method
4.3 MW-assisted synthesis of TMOs
4.4 Conclusion
References
Chapter 5 Solid-state reaction process for metal oxide nanostructures
5.1 Introduction
5.2 Background and motivation
5.3 Solid-state reaction method
5.4 Preliminary treatment
5.5 Applications of metal oxides
5.6 Electrochemical supercapacitors
5.7 Gas sensors
5.8 Conclusions
References
Chapter 6 Solvothermal technique for the synthesis of metal oxide nanostructures
6.1 Introduction
6.2 Historical development of solvothermal process
6.3 Instrumentation details
6.4 Working principle
6.5 Synthesis of various metal oxide nanostructures
6.6 Recent developments in the solvothermal methods
6.7 Advantages and disadvantages
6.8 Conclusions and future perspectives
References
Chapter 7 Hydrothermal method for metal oxide nanostructures
7.1 Introduction
7.2 Historical development
7.3 Operation modes
7.4 Advantages and disadvantages
7.5 Conclusion and future perspectives
References
Chapter 8 Electrospinning of metal oxide nanostructures
8.1 Introduction
8.2 History
8.3 Basic setup and working principles of electrospinning
8.4 Advantages and disadvantages
8.5 Polymer solution properties
8.6 Factor affecting electrospinning
8.7 Electrospinning parameters
8.8 Control of morphology, alignment, and pattern
8.9 Synthesis of different materials by using electrospinning
8.10 Research challenges and limitations
References
Part III Chemical methods of metal oxide film deposition
Chapter 9 Spray-pyrolysis technique for the synthesis of metal oxide nanostructures
9.1 Introduction
9.2 Experimental set up
9.3 Deposition parameters
9.4 Operation mechanism of spray pyrolysis
9.5 Advantages and disadvantages
9.6 Reported metal oxide nanostructures
9.7 Conclusions and future perspectives
Acknowledgment
References
Chapter 10 Successive ionic layer adsorption and reaction (SILAR) method for metal oxide nanostructures
10.1 Introduction
10.2 Basics with and theoretical background
10.3 Operation principle
10.4 Deposition modes
10.5 Synthesis of metal oxides
10.6 Applications
10.7 Advantages and disadvantages
10.8 Conclusions and future perspectives
References
Chapter 11 Electrodeposition of metal oxide nanostructures
11.1 Brief history
11.2 Operation principle
11.3 Electrodeposition of metal oxide nanostructures
11.4 Advantages and disadvantages of electrodeposition method
11.5 Modern applications of electrodeposited metal oxides and future perspectives
Acknowledgments
References
Chapter 12 Electrophoretic deposition of metal oxide nanostructures
12.1 Introduction
12.2 Electrophoretic deposition
12.3 How does a deposit form by EPD?
12.4 Electrophoresis process principle
12.5 Factors influencing on EPD process
12.6 Applications of the electrophoresis deposition
12.7 Conclusion
References
Chapter 13 Chemical bath deposition for metal oxide nanostructures
13.1 Introduction
13.2 Theoretical background
13.3 Experimental details
13.4 Synthesis of MONs
13.5 Applications of metal oxides
13.6 Advantages and disadvantages
13.7 Conclusions and future perspectives
References
Chapter 14 Spin coating/doctor-blading/self-assembly of metal oxide nanostructures
14.1 Introduction
14.2 Thin film deposition techniques
14.3 Spin coating technique
14.4 Technical parameters
14.5 Spin coating with external fields
14.6 Applications
14.7 Advantages
14.8 Limitations
References
Chapter 15 Biogenic synthesis of metal oxide nanostructures
15.1 Introduction
15.2 Zinc oxide
15.3 Copper oxide
15.4 Ferric oxide
15.5 Titanium dioxide nanostructures
15.6 Biosynthesis of cerium oxide or ceria nanostructures
15.7 Silicon dioxide nanostructures
15.8 Conclusions: advantages, disadvantages, and future perspectives
References
Chapter 16 The Langmuir-Blodgett method for metal oxide nanostructures
16.1 Introduction
16.2 Experimental design and essential components
16.3 Synthesis parameters and their significance
16.4 Operation mechanism and theoretical aspects
16.5 Merits and demerits
16.6 Methods for nanoparticle deposition
16.7 Feature scope
References
Chapter 17 Electrochemical synthesis for metal oxide/hydroxide nanostructures
17.1 Introduction
17.2 Experimental set-up
17.3 Parameters in electrochemical synthesis set up
17.4 Working principle
17.5 Techniques for electrochemical synthesis
17.6 Advantages and disadvantages
17.7 Essentials of good electrodeposition
17.8 The development of an electrochemical synthesis
17.9 Electrochemically synthesized metal oxide/hydroxide nanomaterials
17.10 Conclusions and future perspectives
Acknowledgment
References
Index

Rajaram S. Mane

Prof. Rajaram S. Mane received his Ph.D. in Physics from the Shivaji University, Kolhapur, India in 2000 and worked as a postdoctoral fellow at Hanyang University, Korea. He also was on the research faculty of Oxford University, Oxford, UK. Since 2010, he has been a regular professor at the S.R.T.M. University, Nanded, India and a visiting professor of Pusan National University, Korea. His major interests include synthesis of novel nanostructures for energy conversion and storage device technologies.

Affiliations and expertise

Professor, S.R.T.M. University, Nanded, India; Visiting Professor, Pusan National University, Korea

Vijaykumar Jadhav

Dr. Vijaykumar V. Jadhav, MSc, NET, Ph.D. (Physics) is currently working as a Research Scientist at Guangdong Technion, Israel Institute of Technology, Shantou, China. Also he is an Assistant Professor in the Department of Physics, Shivaji College, Udgir, and affiliated with the S.R.T.M. University, Nanded, India and the Applied Nanoscience Group, School of Chemistry, University College of Cork, Ireland. He is a recipient of various prestigious fellowships including a Government of India, Government of Ireland IRC postdoctoral fellowship, where he worked with Prof. Colm O’Dwyer.Dr. Vijaykumar V. Jadhav, MSc, NET, Ph.D. (Physics) is currently working as a Research Scientist at Guangdong Technion, Israel Institute of Technology, Shantou, China. Also he is an Assistant Professor in the Department of Physics, Shivaji College, Udgir, and affiliated with the S.R.T.M. University, Nanded, India and the Applied Nanoscience Group, School of Chemistry, University College of Cork, Ireland. He is a recipient of various prestigious fellowships including a Government of India, Government of Ireland IRC postdoctoral fellowship, where he worked with Prof. Colm O’Dwyer.

Affiliations and expertise

Research Scientist, Guangdong Technion, Israel Institute of Technology, Shantou, China; Assistant Professor, Department of Physics, Shivaji College, Udgir, India

Abdullah M. Al-Enizi

Dr. Abdullah M. Al-Enizi is currently working as an Assistant Professor of Department of Chemistry at the College of Science at King Saud University in Saudi Arabia.

Affiliations and expertise

Assistant Professor, Department of Chemistry, College of Science, King Saud University, Saudi Arabia

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Solution Methods for Metal Oxide Nanostructures

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Rajaram S. Mane

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