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Practical Aspects of Electroorganic Synthesis
- 1st Edition - June 4, 2024
- Authors: Davood Nematollahi, Saber Alizadeh, Ameneh Amani, Sadegh Khazalpour
- Language: English
- eBook ISBN:9 7 8 - 0 - 3 2 3 - 9 5 6 6 7 - 3
Practical Aspects of Electroorganic Synthesis presents an educational insight into the practical aspects of electrosynthesis methods by providing a variety of examples and techn… Read more
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Request a sales quotePractical Aspects of Electroorganic Synthesis presents an educational insight into the practical aspects of electrosynthesis methods by providing a variety of examples and techniques. With the advancement of chemical science and its undeniable role in life, there is a growing need for the employment of green and eco-friendly methods and environmentally acceptable processes to minimize the negative consequences of chemical technologies. These needs and concepts are referred to as “green chemistry” and “sustainable technology”. Electrosynthesis techniques are an example of one of the notable achievements of the interdisciplinary co-operation that assists in minimizing these consequences.
This book comprises three fundamental sections: direct, indirect, and paired electrolysis. As a result, this logically separates the key information needed to conduct electrochemistry into digestible and rational parts. Direct electrolysis discusses anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set up electrochemical experiments. Indirect electrolysis proceeds to explore catalysts and additives in more depth to take on modern electrochemical methods. Finally, this book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products.
Practical Aspects of Electroorganic Synthesis offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques.
- Discusses complete and up-to-date practical concepts of electrosynthesis methods
- Provides sound insights into the experimental approaches of electrosynthesis, covering new and novel synthesis techniques
- Breaks down the fundamentals aspects of electrolysis into three digestible and logical sections
Researchers, academics, undergraduates and scientists within the fields of Analytical Chemistry, Molecular Electrochemistry, Electrosynthesis, Electro-Organic Synthesis, Surface Electrochemistry, Modified Electrode, Green Chemistry and Material science, scientists and researchers within the fields of Laboratory synthesis of Organic-Inorganic Compounds, Industrial synthesis of Organic-Inorganic compounds, Pharmaceutical Industry, Paint Industry, Absorbent and membrane Industry, Fabrication of Energy, Battery, Supercapacitor and Fuel Cell materials. This book can be used for a course as the "Novel and Practical Topics in the Electrochemistry" for Post Graduate Degree and Ph.D students in University
- Cover image
- Title page
- Table of Contents
- Copyright
- Dedication
- About the authors
- Chapter 1. Introduction
- Abstract
- 1.1 Introduction to electrosynthesis
- 1.2 Electrosynthesis methods: direct and indirect methods
- 1.3 Electrosynthesis methods: controlled potential and galvanostatic methods
- 1.4 Electrochemical cells
- 1.5 Electrodes
- 1.6 Solvents
- 1.7 Supporting electrolyte
- 1.8 Green aspects of electroorganic synthesis
- 1.9 Paired electrosynthesis
- 1.10 Cation-pool electrosynthesis
- 1.11 Introduction to electrochemical methods
- References
- Chapter 2. Direct electrosynthesis reactions
- Abstract
- 2.1 Introduction
- 2.2 Bond formation and bond cleavage in direct electrosynthesis
- 2.3 Reductive processes
- 2.4 Summary and conclusions
- References
- Chapter 3. In-direct electrosynthesis reactions
- Abstract
- 3.1 Introduction
- 3.2 Electrocatalyst
- 3.3 Homogeneous electrocatalytic reactions
- 3.4 Heterogeneous electrocatalytic reactions
- References
- Chapter 4. Paired electroorganic synthesis
- Abstract
- 4.1 Introduction
- 4.2 Parallel paired electrosynthesis
- 4.3 Convergent paired electrosynthesis
- 4.4 Divergent paired electrosynthesis
- 4.5 Linear paired electrosynthesis
- 4.6 Other paired electrosynthesis
- 4.7 Summary and conclusions
- References
- Chapter 5. Diels–Alder reaction in electroorganic synthesis
- Abstract
- 5.1 Introduction
- 5.2 Electrochemically induced Diels–Alder reaction via anodic oxidation
- 5.3 Electrochemically induced Diels–Alder reaction via cathodic reduction
- 5.4 Radical cation Diels–Alder reactions by electrocatalysis
- 5.5 Summary and conclusions
- References
- Chapter 6. Michael addition reaction in electroorganic synthesis
- Abstract
- 6.1 Introduction
- 6.2 Electrogeneration Michael acceptor at the anode
- 6.3 Electrogeneration Michael acceptor at the cathode
- 6.4 Summary and conclusions
- References
- Chapter 7. Electrosynthesis of metal-organic frameworks
- Abstract
- 7.1 Introduction
- 7.2 Electrosynthesis of metal-organic frameworks
- 7.3 Electrosynthesis of metal-organic frameworks as powder
- 7.4 Electrosynthesis of metal-organic frameworks as thin film
- 7.5 Mesoporous materials in electrochemistry
- 7.6 Paired electrosynthesis and electrodeposition of metal-organic framework thin films
- 7.7 Summary and conclusions
- References
- Index
- No. of pages: 320
- Language: English
- Edition: 1
- Published: June 4, 2024
- Imprint: Elsevier
- eBook ISBN: 9780323956673
DN
Davood Nematollahi
Davood Nematollahi is a Professor in the Faculty of Chemistry at Bu-Ali Sina University. He completed his PhD with Prof. S. M. Golabi at Tabriz University in 1996 in Electrochemistry. His research is at the intersection of electrochemistry, organic chemistry, and environment chemistry with a focus on fundamental aspects of electroorganic chemistry. He also works on rational design to better understand or discover interesting electrochemical techniques in organic synthesis. He is particularly interested in using green conditions to synthesize of organic compounds. He has published over 400 papers in international journals. In 2012 he was named an ISI highly cited researcher (top 0.1 %). Nematollahi has won several major awards in Iran.
Affiliations and expertise
Professor of Analytical Chemistry, Department of Analytical Chemistry, Faculty of Chemistry and Petroleum Sciences, Bu-Ali Sina University, Hamedan, IranSA
Saber Alizadeh
Saber Alizadeh was born in 1987 in Tabriz, Iran, and received his MSc degree from the Institute for Advanced Studies in Basic Sciences (IASBS) in 2014 for his research on the electrosynthesis and application of mesoporous silica structures under the supervision of Dr. M. Rafiee and Prof. Dr. B. Karimi. He received his PhD degree and a postdoctoral fellowship from Bu-Ali Sina University (BASU) in 2022 for his research on the electrosynthesis and application of metal-organic framework structures under the supervision of Prof. Dr. D. Nematollahi. His research focuses on the application of nanomaterials for electroorganic synthesis, electrocatalysis, and supercapacitors in green conditions. In 2023 he won the Khwarizmi Youth Award and the World Intellectual Property Organization (WIPO) National Award for his research on the design and manufacture of nano-porous catalysts for electrosynthesis of chemical precursors.
Affiliations and expertise
Post.Doc of Analytical Chemistry, Bu-Ali Sina University, IranAA
Ameneh Amani
Ameneh Amani is an Assistant Professor of Analytical Chemistry at Nahavand Higher Education Complex, Bu-Ali Sina University. She obtained her B.Sc. from Damghan University, her M.Sc., and Ph.D. from Bu-Ali-Sina University under the supervision of Professor Davood Nematollahi in 2013. Currently, Amani’s research involves Electrochemistry, Electrosynthesis of organic compounds, and the investigation of electrochemistry of medicinal plants.
Affiliations and expertise
Assistant Professor of Analytical Chemistry, Nahavand Higher Education Complex, Bu-Ali Sina University, Hamedan, IranSK
Sadegh Khazalpour
Sadegh Khazalpour was born in 1986 in Hamedan and obtained his BSc and his MSc from Bu-Ali Sina University with Prof. Davood Nematollahi as the supervisor. During his studies, he completed his thesis on the electrochemical study of 4-(1-piperazino)phenol and resazurin. After that, he became a PhD student in Analytical Chemistry at the University of Bu-Ali Sina under the supervision of Prof. Davood Nematollahi. His research is focused on the electrochemical study of N, N-dimethyl-p-nitrosoaniline, and synthesis of new sulfonamides and electrochemical synthesis of nanoporous mixed ligand metal–organic frameworks: DMOF-1-Zn. He has been a faculty member of Bu-Ali Sina University since 2015.
Affiliations and expertise
Associate prof. of Analytical Chemistry, Department of Analytical Chemistry, Faculty of Chemistry and Petroleum Sciences, Bu-Ali Sina University, Hamedan, IranRead Practical Aspects of Electroorganic Synthesis on ScienceDirect