Organic Functional Group Analysis

Preface

Part I


1. Determination of the Carbonyl Group: Oximation and Other Methods


2. Analysis of Enolic-type Compounds: Kurt Meyer Bromination and Nonaqueous Titration


3. Determination of the Hydroxyl and Amino Groups: Base-catalyzed Acylation Methods


4. Determination of Hydroxyl Groups and Alkoxysilanes: Acid-catalyzed Acetylation Methods


5. Determination of the Epoxide Group: Quantitative Ring Opening Methods


6. Determination of 1,3-Dienes: Diels-Alder Addition Methods


7. Determination of Electron-rich compounds: Electron-Donor-Acceptor Complexes and Charge Transfer Spectra

Part II


1. The Determination of Aldehydes in Oil of Lemon


2. The Estimation of Aldehydes and Ketones by Means of Hydroxylamine


3. Improved Hydroxylamine Method for the Determination of Aldehydes and Ketones. Displacement of Oxime Equilibria by Means of Pyridine


4. Determination of Carbonyl Compounds


5. Macro- and Semi-micro-determination of Aldehydes and Ketones by Reaction with Hydroxyl-ammonium Formate


6. Studies on the Mechanism of Oxime and Semi-carbazone Formation


7. O-methyloximes as Carbonyl Derivatives in Gas Chromatography, Mass Spectrometry, and Nuclear Magnetic Resonance


8. Quantitative Aspects of the Base-catalysed Halogenation of Aliphatic Ketones. Part I. Iodination of Methyl Ketones


9. An improved Kurt Meyer Titration


10. Nuclear Magnetic Resonance Signals from a Tautomeric Mixture


11. Titration of Enols and Imides in Nonaqueous Solvents


12. Quantitative Ester Formation and the Determination of Alcohols and Phenols


13. Determining the Hydroxyl Content of Certain Organic Compounds


14. The Hydrolysis of Acetic Anhydride. Part III. The Catalytic Efficiency of a Series of Tertiary Amines


15. Determination of Hydroxy and Amino Compounds Using Pyromelletic Dianhydride


16. A Study of Base-catalyzed and Salt-catalyzed Acetylation of Hydroxyl Groups


17. The Detection and Estimation of the Relative Amounts of Primary and Secondary Hydroxyl Groups Using N.M.R.


18. Phosphoric Acetylation of the Hydroxyl Group


19. Acid-catalyzed Acetylation of Organic Hydroxyl Groups


20. 1,2-dichloroethane as a Solvent for Perchloric Acid-catalyzed Acetylation


21. Micro Acid-catalyzed Acetylation of Organic Hydroxyl Groups


22. Determination of Alkoxy Groups in Alkoxysilanes by Acid-catalyzed Acetylation


23. Epoxy Acids from Oleic and Elaidic Acids


24. Direct Titration of Oxirane Oxygen with Hydrogen Bromide in Acetic Acid


25. Direct Titration of Epoxy Compounds and Aziridines


26. An Improved Direct Titration and α-epoxy Compounds Using Crystal Violet as the Indicator


27. The Volumetric Determination of Anthracene with Maleic Anhydride


28. Determination of Diels-Alder Active Dienes with Tetracyanoethylene


29. Precise Determination of the Molecular Weight of Trinitrobenzene Complexes


30. A Study of the π Complexes of Tetracyanoethylene with Phenols, Aromatic Hydrocarbons and Aryl Ethers


31. Diphenylpicrylhydrazyl as an Organic Analytical Reagent in the Spectrophotometry Analysis of Phenols

Index