Metal-Organic Frameworks in Analytical Sample Preparation and Sensing
- 1st Edition - June 25, 2024
- Editors: Verónica Pino, Jorge Pasán, Maria José Trujillo Rodríguez
- Language: English
- Paperback ISBN:9 7 8 - 0 - 4 4 3 - 1 8 9 7 1 - 5
- eBook ISBN:9 7 8 - 0 - 4 4 3 - 1 8 9 7 2 - 2
Metal-organic Frameworks in Analytical Sample Preparation and Sensing presents all the areas of applications of metal-organic frameworks in analytical sample preparation. Metal-org… Read more
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Request a sales quoteMetal-organic Frameworks in Analytical Sample Preparation and Sensing presents all the areas of applications of metal-organic frameworks in analytical sample preparation. Metal-organic frameworks are crystalline coordination polymers with robust and stable crystal structures, high synthetic tunability, and interesting properties for their use in analytical applications, including their detailed use as sorbents in miniaturized-extraction procedures and as components in sensors.
This book also provides important information about the synthesis and characterization of these materials, with useful tips written by experts on the subject with respect to their conditioning, handling, and recycling. Their outstanding properties, adsorptive capabilities, and structural diversity are also highlighted. This will help experts in the field to select the proper metal-organic framework for a particular analytical application.
- Provides analytical scientists with a unified reference guide for the use of metal-organic frameworks in miniaturized-extraction methods and sensing.
- Covers aspects related to the development, characterization, conditioning and handling of metal-organic frameworks. Issues of scale-up will be covered too.
- Addresses the proper metal-organic framework for a particular analytical miniaturized method.
Academics but also Analytical Scientists and Laboratory Technicians primary related to the food, environmental, and bioanalysis sectors.
- Cover image
- Title page
- Table of Contents
- Copyright
- List of contributors
- Acknowledgments
- Section I: Reticular materials: synthesis, characterization, and properties
- Chapter 1. Introduction and general aspects of metal-organic frameworks and other novel reticular materials
- Abstract
- 1.1 Interest of reticular materials
- 1.2 Historical development of metal- and covalent-organic frameworks
- 1.3 Metal-organic frameworks: generic aspects and considerations for their applicability in analytical chemistry
- 1.4 Covalent-organic frameworks: generic aspects and considerations for their applicability in analytical chemistry
- 1.5 Adequate characterization of MOFs and COFs: X-ray diffraction and adsorption techniques
- 1.6 Analytical chemistry applications of MOFs and COFs
- 1.7 Conclusion
- Acknowledgments
- References
- Chapter 2. Synthesis of metal-organic frameworks with interest in analytical chemistry
- Abstract
- 2.1 Introduction
- 2.2 General concepts
- 2.3 New synthesis approach
- 2.4 MOF synthesis with interest in the electrochemical sensor
- 2.5 MOF synthesis with interest in the separation and sample preparation
- 2.6 Summary and outlook
- References
- Chapter 3. Synthesis of composites based on reticular materials with interest in analytical chemistry
- Abstract
- 3.1 Introduction
- 3.2 Reticular materials and nanoparticles composites
- 3.3 Reticular materials and polymers composites
- 3.4 Reticular materials and molecularly imprinted polymers composites
- 3.5 Reticular materials and carbonaceous materials composites
- 3.6 Other composites based on reticular materials
- 3.7 Composites characterization
- 3.8 Conclusions
- Note
- Acknowledgments
- Abbreviations
- References
- Section II: Metal-organic frameworks as sorbents in analytical sample preparation
- Chapter 4. Metal-organic frameworks in micro solid-phase extraction
- Abstract
- 4.1 Introduction
- 4.2 Bare MOFs in µ-SPE applications
- 4.3 MOF-based composites in µ-SPE applications
- 4.4 Conclusions
- Acknowledgments
- References
- Chapter 5. Metal-organic frameworks in micro-dispersive solid-phase extraction and stir bar sorptive extraction
- Abstract
- 5.1 Introduction
- 5.2 Sorbent-based extraction methods
- 5.3 The application of MOFs in μ-DSPE
- 5.4 The application of MOFs in SBSE
- 5.5 Conclusions and outlooks
- References
- Chapter 6. Metal-organic frameworks in magnetic-based methods
- Abstract
- 6.1 Introduction to magnetic solid-phase extraction
- 6.2 Strategies for the implementation of metal-organic frameworks as sorbents for MSPE
- 6.3 Conclusions
- References
- Chapter 7. Metal-organic frameworks in solid-phase microextraction
- Abstract
- 7.1 Solid-phase microextraction (SPME): on-fiber and in-tube
- 7.2 Methods for SPME coatings preparation
- 7.3 Application of MOFs in SPME
- 7.4 Conclusion and future remarks
- References
- Chapter 8. Metal-organic frameworks in thin film microextraction
- Abstract
- 8.1 Thin films: general overview
- 8.2 TF solid-phase microextraction
- 8.3 Preparation of MOF-TFs
- 8.4 MOFs-TFs in TFME
- 8.5 Applications of MOF-TFs in TFME
- Abbreviations
- References
- Chapter 9. Hyphenating microextraction using metal-organic frameworks with separation and detection techniques
- Abstract
- 9.1 Introduction
- 9.2 Flow-through microextraction techniques
- 9.3 Batch microextraction techniques
- 9.4 Conclusions and future perspectives
- Acknowledgments
- Abbreviations
- References
- Section III: Metal-organic frameworks as sensors for analysis
- Chapter 10. Metal-organic frameworks as luminescent sensors
- Abstract
- 10.1 Introduction
- 10.2 Luminescence in metal-organic frameworks
- 10.3 Designing of LMOFs
- 10.4 Detection of hazardous organic pollutants
- 10.5 Summary
- 10.6 Conclusion and outlook
- Acknowledgments
- References
- Chapter 11. Metal-organic frameworks as electrochemical sensors
- Abstract
- 11.1 Introduction
- 11.2 Metal-organic framework-based electrochemical sensors for analytes from liquid phase
- 11.3 Metal-organic framework-based electrochemical sensors for analytes from gas phase
- 11.4 Summary and outlook
- References
- Section IV: Novel reticular materials in analytical sample preparation and sensing synthesis and applications of covalent-organic frameworks in analytical chemistry
- Chapter 12. Synthesis of covalent-organic frameworks and applications in analytical chemistry
- Abstract
- 12.1 Introduction
- 12.2 Design and synthesis of covalent-organic frameworks
- 12.3 Application of covalent-organic frameworks as sorbents in sample preparation
- 12.4 Conclusions
- Acknowledgments
- References
- Chapter 13. Covalent-organic frameworks for luminescent sensors
- Abstract
- 13.1 Introduction
- 13.2 Explosives
- 13.3 Heavy metals
- 13.4 Biological molecules
- 13.5 pH
- 13.6 Volatile organic compounds (VOCs), amines and water
- 13.7 Conclusion and future perspectives
- 13.8 Funding Sources
- References
- Index
- No. of pages: 432
- Language: English
- Edition: 1
- Published: June 25, 2024
- Imprint: Elsevier
- Paperback ISBN: 9780443189715
- eBook ISBN: 9780443189722
VP
Verónica Pino
Dr. Pino is Professor at University of La laguna, and PI of Laboratory of Materials for Chemical Analysis (MAT4LL). She obtained her PhD in Chemistry from Universidad de La Laguna (Spain) in 2002 with Doctorate Extraordinary Award and Special Mention for Young Canary Researchers from the Canary Government. She has conducted several research stays, including Wake Forest University, Canary Institute of Agrarian Research, Iowa State University, The University of Toledo, and University Claude Bernard. She was awarded with a prestigious “Ramón y Cajal” research associate position in 2010 at ULL. She has published over 120 JCR research articles included within JCR, 25 book chapters, an h-index of 39, and over 4800 citations. She has been editor of 5 books of Wiley related to Analytical Separation Science, and has been PI of 5 research consecutive projects with funding of the Spanish Government.
Affiliations and expertise
Professor, University of La laguna and PI of Laboratory of Materials for Chemical Analysis (MAT4LL), SpainJP
Jorge Pasán
Dr. Pasán is Distinguished Researcher at University of La laguna, and member of Laboratory of Materials for Chemical Analysis (MAT4LL). He obtained his PhD in Physics in 2006, obtaining the Doctorate Extraordinary Award. He has performed research stays in Lawrence Berkeley National Laboratory (USA), European Synchrotron Radiation Facility (France), and Instituto de Ciencia Molecular (Valencia, Spain). She has published more than 150 research publications, and 1 book chapters, with an h-index of 41 and over 4700 citations. He has been participated in more than 10 research projects with funding of the Spanish Government, and he is Academic Editor of Nanomaterials.
Affiliations and expertise
Distinguished Researcher, University of La laguna, SpainMT
Maria José Trujillo Rodríguez
Dr. Trujillo-Rodríguez is a Junior Researcher at University of La laguna, and member of Laboratory of Materials for Chemical Analysis (MAT4LL). She obtained her PhD in Chemistry in 2017, obtaining the Doctorate Extraordinary Award. She has worked as researcher in Iowa State University (USA), Universitat de les Illes Balears (Spain), and Consejo Superior de Investigaciones Científicias (CSIC, Spain), and is performing a research stay at Universidade de Aveiro (Portugal). She has published 29 research publications, and 7 book chapters. These publications generated more than 950 citations and h-index of 16. She has collaborated in 9 different research projects. In 2014, she obtained the SPME user club Award of Sigma Aldrich.
Affiliations and expertise
Junior Researcher, University of La laguna and member of Laboratory of Materials for Chemical Analysis (MAT4LL), SpainRead Metal-Organic Frameworks in Analytical Sample Preparation and Sensing on ScienceDirect