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Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis
- 1st Edition - October 22, 2024
- Editors: Rajeev Jain, Abuzar Kabir
- Language: English
- Paperback ISBN:9 7 8 - 0 - 4 4 3 - 1 3 9 0 7 - 9
- eBook ISBN:9 7 8 - 0 - 4 4 3 - 1 3 9 0 6 - 2
Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis provides a comprehensive overview of GAMs in forensic drug analysis, including… Read more
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Request a sales quoteGreen Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis provides a comprehensive overview of GAMs in forensic drug analysis, including green sample preparation techniques, in-situ analytical platforms (such as DIC and µPADs), and on-site sample preparation. The book discusses not only eco-friendly GAM’s, but also methods which provide high sample throughput and cost-effective analysis, and are therefore of immense use in resource limited laboratories of developing countries. This is a comprehensive source of literature for analytical scientists in this developing area of sustainable and affordable analytical methods.
- Provides a comprehensive overview of GAMs in forensic drug analysis, including green sample preparation techniques, in-situ analytical platforms (such as DIC and µPADs) and on-site sample preparation
- Presents scientific data for synthesis and application of green solvents (e.g., DES and ILs) and adsorbents (e.g., FPSE membranes)
- Offers method development, optimization, and validation strategies for GAMs
Analytical chemists, Forensic toxicologists, clinical toxicologists, forensic chemists, analytical toxicologists, Academicians and researchers, Post-graduate and research students, Pharmaceutical industries, application scientists, technicians involved in drug testing laboratories, attorneys involved in drug analysis litigations, policy makers
- Title of Book
- Cover image
- Title page
- Table of Contents
- Copyright
- Dedication
- List of contributors
- Preface
- Section A: Green analytical methods
- Chapter 1. Green analytical methods and principles of green analytical chemistry
- Abstract
- 1.1 Introduction
- 1.2 History of the “green” concept in chemistry
- 1.3 Green profile evaluation using the last accepted tools
- 1.4 Green analytical methods
- 1.5 Conclusions
- References
- Further reading
- Chapter 2. Green analytical chemistry metrics
- Abstract
- 2.1 Introduction
- 2.2 National Environmental Method Index
- 2.3 Analytical Eco-Scale
- 2.4 Green Analytical Procedure Index
- 2.5 Analytical Greenness calculator
- 2.6 Complementary Green Analytical Procedure Index
- 2.7 Analytical Greenness metric for sample preparation
- 2.8 Sample preparation metric of sustainability
- 2.9 Conclusion
- Acknowledgment
- References
- Section B: Miniaturized sorbent-based techniques in forensic drug analysis
- Chapter 3. Fabric phase sorptive extraction: a new generation green sample preparation technique
- Abstract
- 3.1 Introduction
- 3.2 Principle and theory of fabric phase sorptive extraction extraction
- 3.3 Sol–gel fabric phase sorptive extraction membrane creation procedure
- 3.4 Chemistry of fabric phase sorptive extraction sorbents
- 3.5 Fabric phase sorptive extraction procedure
- 3.6 Applications of fabric phase sorptive extraction for the extraction of drugs from complex biological samples
- 3.7 Factors affecting the extraction efficiency of fabric phase sorptive extraction
- 3.8 Conclusion
- References
- Chapter 4. Solid-phase microextraction
- Abstract
- 4.1 Introduction
- 4.2 Green analytical sample preparation approach
- 4.3 Solid-phase microextraction: modes and configurations
- 4.4 Forensic applications of solid-phase microextraction with gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry
- 4.5 Different matrices for solid-phase microextraction in forensic analysis
- 4.6 Miniaturization and high throughput
- 4.7 Rapid analysis
- 4.8 Conclusion
- References
- Chapter 5. Microextraction by packed sorbent
- Abstract
- 5.1 Theory
- 5.2 Configurations and sorbents
- 5.3 Extraction process
- 5.4 Advantages and drawbacks
- 5.5 Applications
- 5.6 Applications in forensic toxicology
- 5.7 Future perspectives and conclusions
- Acknowledgments
- References
- Chapter 6. Matrix solid-phase dispersion
- Abstract
- 6.1 Introduction
- 6.2 Matrix solid-phase dispersion principles
- 6.3 Latest developments
- 6.4 Solvents
- 6.5 New elution solvents
- 6.6 New modes of matrix solid-phase dispersion extraction
- 6.7 Challenges and future perspectives
- 6.8 Conclusion
- References
- Chapter 7. Stir-bar sorptive extraction
- Abstract
- 7.1 Introduction
- 7.2 Stir-bar sorptive extraction principles
- 7.3 Stir-bar sorptive extraction steps
- 7.4 Stir-bar sorptive extraction: advantages, limitations, and automation
- 7.5 Novel coatings
- 7.6 Derivatization
- 7.7 Stir-bar sorptive extraction applications in forensic drug analysis
- 7.8 Conclusions
- References
- Chapter 8. Disposable pipette extraction
- Abstract
- Glossary
- Abbreviations
- Key points/objectives box
- 8.1 Introduction
- 8.2 Operation of disposable pipette extraction: disposable tips
- 8.3 Experimental optimization with disposable pipette extraction disposable tips
- 8.4 Advantages and disadvantages
- 8.5 Types of disposable pipette extraction tips
- 8.6 Applications
- 8.7 Conclusion
- References
- Chapter 9. Sorbent materials based on cellulosic substrates
- Abstract
- 9.1 Contextualization
- 9.2 General synthetic approaches
- 9.3 Paper-based sorptive phases
- 9.4 Cotton-based sorptive phases
- 9.5 Wood-based sorptive phases
- 9.6 Cork-based sorptive phases
- 9.7 Cellulose cone tips as sorptive phases
- 9.8 Conclusions
- References
- Chapter 10. Metal-organic framework-based microextraction
- Abstract
- 10.1 Introduction
- 10.2 Synthesis of metal-organic frameworks
- 10.3 Characterization of metal-organic frameworks
- 10.4 Applications of metal-organic frameworks in microextraction
- 10.5 Conclusions
- References
- Section C: Miniaturized solvent based techniques in forensic drug analysis
- Chapter 11. Single-drop microextraction
- Abstract
- 11.1 Introduction
- 11.2 Single drop microextraction revisited
- 11.3 New configurations and automation
- 11.4 Novel solvents in single drop microextraction
- 11.5 Nanoparticles in single drop microextraction
- 11.6 Method optimization approaches
- 11.7 Green analytical chemistry metrics
- 11.8 Applications of single drop microextraction
- 11.9 Conclusions and future prospects
- Acknowledgment
- References
- Chapter 12. Dispersive liquid-liquid microextraction for forensic drug analysis
- Abstract
- 12.1 Introduction
- 12.2 DLLME principle
- 12.3 DLLME in forensic drug analysis
- 12.4 Modifications to DLLME
- 12.5 Conclusion and future perspective
- References
- Chapter 13. Green solvent microextraction
- Abstract
- 13.1 Introduction
- 13.2 Green chemistry
- 13.3 Green solvents
- 13.4 Liquid-based microextraction procedures
- 13.5 Conclusions
- References
- Chapter 14. Deep eutectic solvents in forensic drug analysis
- Abstract
- 14.1 Introduction
- 14.2 Fundamentals, preparation, and characterizations of deep eutectic solvents
- 14.3 Recent applications of deep eutectic solvents in microextraction techniques for the analysis of forensic drugs
- 14.4 Trends in deep eutectic solvents-based microextraction approaches in forensic drug analysis
- 14.5 Conclusions
- References
- Chapter 15. Sustainable approaches to green derivatization in chemical analysis
- Abstract
- Abbreviations
- 15.1 Introduction
- 15.2 Approaches to green derivatization
- 15.3 Conclusion
- References
- Chapter 16. Automatic microextraction methods for forensic drugs analysis: principles, recent trends, challenges, and applications
- Abstract
- Abbreviations
- 16.1 Introduction
- 16.2 Basic approaches to automation of microextraction techniques
- 16.3 Applications in forensic drug analysis: selected examples
- 16.4 Recent trends in automatic methods: prospects
- 16.5 Conclusions
- References
- Section D: Green analytical methods for on-site and in-situ forensic drug analysis
- Chapter 17. Microfluidic paper-based analytical devices
- Abstract
- 17.1 Introduction
- 17.2 Microfluidic paper-based analytical devices
- 17.3 Applications of microfluidic-paper based in toxicology
- 17.4 Conclusion remarks
- References
- Chapter 18. The role of digital image colorimetry in drug analysis
- Abstract
- 18.1 Introduction
- 18.2 Fundamentals and operational requirements of digital image colorimetry
- 18.3 Applications of digital image colorimetry in drug analysis
- 18.4 Conclusion and future trends
- References
- Chapter 19. On-site analytical techniques for forensic chemistry
- Abstract
- 19.1 Introduction
- 19.2 On-site analytical techniques
- 19.3 Concluding remarks
- Acknowledgments
- References
- Index
- No. of pages: 556
- Language: English
- Edition: 1
- Published: October 22, 2024
- Imprint: Elsevier
- Paperback ISBN: 9780443139079
- eBook ISBN: 9780443139062
RJ
Rajeev Jain
Dr. Rajeev Jain is Senior Scientist (Forensic Toxicology) at Central Forensic Science Laboratory, Ministry of Home Affairs, Govt. of India. He has more than 15 years of research experience in the field of analytical toxicology. During his tenure as Forensic Toxicologist, he has examined post-mortem samples of more than 1000 medico-legal cases pertaining to drug overdose and poisoning. He has obtained his Ph.D. degree in Analytical Toxicology from CSIR-Indian Institute of Toxicology Research (India). His research work is focused on Development of sustainable, affordable, and green analytical methods based on microextraction techniques for the determination of chemical analytes for forensic toxicological, clinical, and environmental importance in various complex samples.
Affiliations and expertise
Senior Scientist (Forensic Toxicology), Central Forensic Science Laboratory, Ministry of Home Affairs, Govt of India, Chandigarh, IndiaAK
Abuzar Kabir
Dr. Abuzar Kabir is a Research Associate Professor in the Department of Chemistry and Biochemistry at Florida International University, Miami, Florida, USA. His research focusses on the synthesis, characterization and applications of novel sol-gel derived advanced material systems to be used as chromatographic stationary phases, surface coatings of high-efficiency microextraction sorbents, nanoparticles, microporous and mesoporous functionalized sorbents, molecularly imprinted polymers for analysing trace and ultra-trace level concentration of polar, medium polar, nonpolar, ionic analytes, heavy metals, and organometallic pollutants from complex sample matrices.
Affiliations and expertise
Research Associate Professor, Florida International University, Department of Chemistry and Biochemistry, Florida International University, USARead Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis on ScienceDirect