Determination Of Organic Structures By Physical Methods V6

List of Contributors

Preface

Contents of Other Volumes


1. Amino Acid Sequencing of Oligopeptides by Mass Spectrometry

I. Introduction

II. Electron Impact Fragmentation of Derivatized Oligopeptides

III. Chemical Ionization of Derivatized and Underivatized Oligopeptides

IV. Field Desorption Ionization of Underivatized Oligopeptides

V. Derivatization Methods

VI. Analytical Techniques

VII. The Future of Mass Spectrometry for Peptide Sequencing

References


2. Computerized Structure Retrieval and Interpretation of Mass Spectra

I. Introduction

II. Inductive Approaches

III. Deductive Approaches

IV. The Combination Approaches

References


3. Flash Photolysis and Structure

I. Introduction

II. Instrumentation

III. Spectra of Free Radicals

IV. Electronic Structure of Excited States

V. Some Applications to Photobiological Systems

VI. Summary

References


4. 29Si Nuclear Magnetic Resonance

I. Introduction

II. 29Si Chemical Shifts

III. 29Si Spin-Spin Coupling Constants

IV. Relaxation and the Nuclear Overhauser Effect

References


5. The Nuclear Overhauser Effect

I. Introduction

II. Theory

III. Experimental Methods

IV. Chemical Applications

V. The Effects of Chemical Exchange and Internal Motion

References


6. Molecular Structures by NMR in Liquid Crystals

I. Introduction

II. The Liquid Crystals

III. Experimental Methods

IV. Spectral and Structural Analysis

V. Examples of Structural Determinations

Appendix

References

Author Index

Subject Index