Comprehensive Sampling and Sample Preparation
- 2nd Edition - June 1, 2025
- Editor: Mustafa Soylak
- Language: English
- Hardback ISBN:9 7 8 - 0 - 4 4 3 - 1 5 9 7 8 - 7
- eBook ISBN:9 7 8 - 0 - 4 4 3 - 1 5 9 7 9 - 4
Comprehensive Sampling and Sample Preparation, Second Edition, Four Volume Set is a complete treatment of the theory and methodology of sampling in all physical phases and the t… Read more
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Request a sales quoteComprehensive Sampling and Sample Preparation, Second Edition, Four Volume Set is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. Emerging areas in the field are discussed in-depth and contributions are organized to reflect the way in which analytical chemists approach a problem.
The latest edition includes updated chapters along with new chapters on exciting topics including micro- and nano extractions, green solvents, nanomaterials, nanocomposites in extraction studies, and solid-phase extractions. This work will appeal to a broad audience of analytical chemists. It will also assist educators and practitioners in the preparation of courses and to spark students’ interest in sampling and sample preparation.
- Covers the entire scope of modern extraction techniques
- Contains concisely written, consistently formatted chapters to efficiently provide information
- Compiles knowledge from a global team of experts and takes an interdisciplinary approach
- Theoretical Approaches
- Methodologies for Sample Preservation & Stabilization
- Assessing and Controlling Sample Contamination
- Sample Homogenization
- Sampling Strategy for Process Control
- Integrated Total Analysis Systems
- Nanomaterials
- Indoor Air Sampling
- Exposure Assessment in the Workplace
- Aerosols PM2.5 and PM10
- Passive Sampling of Atmospheric Organic Contaminants
- Equipment for Water Sampling Including Sensors
- Passive Sampling of Organic Contaminants in Waters
- Application of IoT for Sensing
- Passive Sampling for Inorganic Contaminants in Water
- Sampling of Organic Contaminants from Seawater
- Sampling Approaches for Trace Element Determination in Seawater
- Sampling of Humic and Colloidal Phases in Liquid Samples
- Sampling of Fish, Benthic Species, and Seabird Eggs in Pollution Assessment
- Trends and Perception Towards Collection and Preparation of Human Biological Specimens for Contaminant Analysis
- Food Contaminants
- Legal and Forensic Sampling
Section 2: Theory of Extraction Techniques
- Theory of Extraction
- Headspace Analysis
- Liquid–Liquid Extraction: Basic Principles and Automation
- Soxhlet Extraction and New Developments (Soxtec)
- Soxhlet vs ASE: Principles and Practice
- Accelerated Solvent Extraction (ASE) and High-Temperature Water Extraction
- Fundamentals of Supercritical Fluid Extraction
- Microwave-Assisted Extraction
- Liquid-Phase Microextraction
- Dispersive Liquid-Liquid Microextraction
- Ionic Liquids and Derivatives in (Micro)Extraction Strategies
- Sorbent Chemistry, Evolution
- Sorbents for Air Sampling and Analysis
- Principles and Practice of Solid-Phase Extraction
- Matrix Solid Phase Dispersion
- Sol-Gel Materials in Analytical Microextraction
- Molecularly Imprinted Polymers
- Monoliths, Fundamentals for Sample Preparation
- Bioaffinity Sorbents
- Nanomaterials for Sample Preparation: Overview of Recent Innovative Strategies
- Solid Phase Microextraction
- Membrane Extraction: General Overview and Techniques
- Hollow Fiber Liquid-Phase Microextraction (HF-LPME)
- Microdialysis Sampling in the Brain: Analytical Approaches and Challenges
- Recent Developments on the Design of Advanced Porous Materials Based on Metal-Organic Frameworks (MOFs), Covalent Organic Frameworks (COFs), and Their Combinations into Composites as Sorbents in Sample Preparation and Chromatographic Applications
- Fundamentals of Electro-Driven Sample Preparation
- Analytical Derivatization Techniques
- Sample Preparation Automation for GC Injection
- LC Automation
- Online Column-Switching Sample Preparation for Liquid Chromatography
- Fundamentals and Applications of Needle Trap Devices
- Validation and Regulatory Issues for Sample Preparation
- Sample Preparation Strategies for Direct Analysis by Mass Spectrometry
- Sample Preparation for Lab-on-a-Chip / Microfluidic Sample Preparation
- Fundamentals of In Vivo Sampling
- Sample Preparation Methods in Bottom-Up Proteomics
- Current Advances in On-Site Environmental Microextraction Techniques
- Green Analytical Chemistry in Sample Preparation
- Deep Eutectic and Natural Deep Eutectic Solvents in Sample Preparation
- Supramolecular Solvents in Sample Preparation
- Fundamentals of Switchable Solvent-Based Extractions
- Natural Sorbents for Green Sample Preparation
Section 3: Extraction Techniques and Applications: Biological/Medical/Environmental/Forensics
- General Considerations When Dealing with Biological Fluid Samples
- Comprehensive Insight on Managing Tissues and Cell Samples with Tissue Banking Practices
- Cell Separation, Perfusion from Tissue, Organelle Fractionation, etc.
- Tissue Preparation for Microscopy and Histology
- Blood Sample Collection and Handling
- Urine Sample Collection and Handling
- DNA Damage, Repair, and Genome Instability
- Proteolytic Digestion Methods for Shotgun Proteomics
- Microwave Digestion of Protein Samples for Proteomics Applications
- Sample Preparation for Glycoproteins
- Sampling and Sample Preparation for LC-MS-Based Metabolomics of Samples of Mammalian Origin
- Tissue, Serum, and Saliva Sampling for Proteomic Analysis
- Pre-Concentration and Sample Treatment Techniques for Trace Element Analysis
- Enzymatic Treatment of Biological Samples for Speciation Analysis
- Enzyme Digestion for Speciation of Arsenic
- Chromium Speciation
- Mercury Speciation and Binding to Biomacromolecules
- Bioaccessibility Extractions for Contaminant Risk Assessment
- Application of SPME to Pharmacodynamics, Pharmacokinetics, and Toxicology
- Electrospun Nanofiber-Based Solid-Phase Microextraction Media
- Sample Preparation of Complex Biological Samples in the Analysis of Trace-Level Contaminants
- Sorbent-Phase Sample Preparation in Environmental Analysis
- Recent Advances in Sample Preparation for Pesticide Analysis
- Sample Pretreatment Techniques for Per- and Polyfluoroalkyl Substances (PFAS)
- Recent Advances in Solid-Phase Microextraction for Environmental Applications
- Environmental Applications of Cloud-Point Extraction
- Sample Preparation for Food Contaminant Analysis
- Liquid-Based Microextraction Techniques for Environmental Analysis
- Sample Preparation for Chromatographic Applications in Forensic Science
- Recent Advances in Solid-Phase Microextraction for Forensic Applications
- Recent Advances in Sample Preparation for Explosives
- Chemical Warfare Agents: Development and Applications of Sample Preparation Approaches
- Applications of Needle-Type Sample Preparation Devices for Environmental and Natural Samples
- Use of Unconventional Solvents for Sample Preparation in Environmental Analysis
- Advances in the Field of Preparative Gas Chromatography for the Enrichment and Isolation of Key Volatiles
Section 4: Extraction Techniques and Applications: Food and Beverage
- Headspace Sampling in Flavor and Fragrance Field
- Sampling and Sample Preparation Methods for the Determination of the Volatile Components of Milk and Dairy Products
- Sampling Techniques for the Determination of Volatile Components in Food of Animal Origin
- Sampling Techniques for the Determination of the Volatile Fraction of Honey
- Sample Preparation for Food Flavors Analysis
- Extraction Techniques for the Determination of Phenolic Compounds in Food
- Extraction Techniques for the Determination of Carotenoids and Vitamins in Food
- Sample Preparation Techniques for the Determination of Fats in Food
- Sample Preparation for the Determination of Carbohydrates in Food and Beverages
- Solvent-Based Extraction Techniques for the Determination of Pesticides in Food
- Advances in Magnetic Sorbents for Extracting and Measuring Pesticides in Food Samples
- Sample Preparation Techniques for the Determination of Some Food Contaminants (Polycyclic Aromatic Hydrocarbons, Mineral Oils, and Phthalates)
- Sampling and Sample Preparation Techniques for the Determination of Mycotoxins in Food Matrices
- Sample Preparation Techniques for the Determination of Veterinary Drugs in Food Matrices
- Application of Subcritical and Supercritical Fluid Extraction in Food Processing
- Applications of SPE-MIP in the Field of Food Analysis
- Application of Stir-Bar Sorptive Extraction in Food Analysis
- Sample Preparation for the Determination of Metals in Food Samples
- Membrane-Based Extraction Techniques in Food Analysis
- Dispersive Solid-Phase Extraction of Water-Soluble Synthetic Colorants in Beverages
- The Use of Composites for Magnetic Solid Extraction in Beverage and Food
- Solid-Phase Extraction for Determination of Phenolic Compounds in Food and Beverage
- Solid-Phase Extraction for the Determination of Vitamins in Food and Beverages
- Dispersive Solid-Phase Microextraction of Organic and Inorganic Analytes in Food and Beverage
- Microextraction of Food Colorants in Soft Drinks, Candies, and Pastilles
- Dispersive Liquid–Liquid Microextraction of Organic and Inorganic Analytes in Food and Beverage
- Headspace Solid-Phase Microextraction of Alcoholic Beverages and Fermented Foods
- Microextraction in Food and Beverage: Applications of Liquid-Liquid Microextraction
- Use of Hydrogen Extraction in the Food Industry
- No. of pages: 3500
- Language: English
- Edition: 2
- Published: June 1, 2025
- Imprint: Academic Press
- Hardback ISBN: 9780443159787
- eBook ISBN: 9780443159794
MS
Mustafa Soylak
Prof. Dr. Mustafa Soylak is working on Environmental Analytical Chemistry, Nanotechnology, Nanomaterials, Nanocomposites, and Separation/ Preconcentration Techniques including Solid Phase Extraction, Coprecipitation, Cloud point extraction, membrane filtration, speciation and microextraction of trace organic and inorganic species. Dr. Soylak has an h-index of 111 (Web of Science). He has over 750 papers in Web of Science, 8 book chapters and reviews, two textbooks (in Turkish), and one textbook on microextraction techniques (Elsevier, 2020). He is the Editor-in-Chief of Comprehensive Sampling and Sample Preparation (Elsevier, 2022). He was a visiting professor at King Saud University- Saudi Arabia in 2010-2016 and at Near East University on 2018 to 2019. He is now a Professor at Erciyes University, Department of Chemistry, Kayseri-Turkey. He is the editorial board member of the Journal of Hazardous Materials, International Journal of Environmental Analytical Chemistry, Arabian Journal of Chemistry, Turkish Journal of Chemistry, and Journal of Nanostructure in Chemistry. He received TUBITAK (Turkish Scientific and Technological Research Council) Encouragement Award in 2001. He is the recipient of the highest prestigious science award in Turkey, the TUBITAK Science Award in 2020. He won also İlim Yayma Award from the İlim Yayma Foundation in 2021. He has been a principal member of the Turkish Academy of Sciences (TUBA) since 2020. He has obtained a TÜBİTAK 2247-A National Fellowship for Outstanding Researchers (2021). He published more than 750 research papers.