Analytical Methods for Coal and Coal Products
Volume II
- 1st Edition - January 28, 1979
- Imprint: Academic Press
- Editor: Clarence Karr
- Language: English
- Paperback ISBN:9 7 8 - 1 - 4 8 3 2 - 4 1 3 2 - 6
- Hardback ISBN:9 7 8 - 0 - 1 2 - 3 9 9 9 0 2 - 3
- eBook ISBN:9 7 8 - 1 - 4 8 3 2 - 7 3 1 6 - 7
Analytical Methods for Coal and Coal Products, Volume II, aims to provide a detailed presentation of what constitutes the first comprehensive reference work devoted exclusively to… Read more
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Analytical Methods for Coal and Coal Products, Volume II, aims to provide a detailed presentation of what constitutes the first comprehensive reference work devoted exclusively to the subject of analytical methodology for coal and coal products. The various chapters have been arranged according to either a specific coal process or a specific coal use problem. The topics discussed include the structure of coal and coal products, minerals in coal, coal carbonization products, and coal combustion products. The general philosophy of this work is to strike a balance between sophisticated analyses based on expensive instrumentation such as mass or nuclear magnetic resonance spectrometers, and the more common, less expensive equipment typically employed in the standard methods. Likewise there is an attempt to strike a balance between the expertise available from within the United States and that found in other countries, offering a broader viewpoint. Altogether, a large number of cross references have been entered in these chapters to enable the reader to make maximum use of pertinent information in all of the chapters.
List of Contributors
Preface
Contents of Volume I
Part V Structure of Coal and Coal Products
Chapter 20 Analysis of the Organic Substance of Coals: Problems Posed by the Presence of Mineral Matter
I. Introduction
II. Reactivity of Coal Mineral Matter
III. Definitions of Ultimate Analyses
IV. Information Required for a dmmf Analysis
V. Optimum and Approximate Procedures for Computing dmmf Analyses
VI. The Problem of Organic Oxygen
VII. Participation by Mineral Matter in Reactions of the Organic Substance of Coals
References
Chapter 21 Analysis of Organic Compounds Trapped in Coal, and Coal Oxidation Products
I. Introduction
II. Analytical Methods
III. Analysis of Trapped Organic Compounds in Coals and Pyrolysis Products
IV. Analysis of Oxidation Products
V. Determination of Aromaticity of Coal by Fluorination
References
Chapter 22 Assessment of Structures in Coal by Spectroscopic Techniques
I. Introduction
II. Spectroscopic Techniques
III. Assessment of Coal Structure
References
Chapter 23 Nuclear Magnetic Resonance Spectroscopy
I. Introduction
II. Theory of Nuclear Magnetic Resonance
III. Experimental Methods
IV. Interpretation of Spectra
V. Selected Applications of NMR to Coal and Coal Products
VI. Conclusion
References
Chapter 24 High Resolution 1H-, 2H-, and 13C-NMR in Coal Research
I. Introduction
II. Experimental Methods
III. The Determination of Carbon Aromaticity
IV. Estimation of Mean Structural Units
V. 13C-NMR—Improvements in Resolution, 1968-1977
VI. Applications
VII. Summary and Prognosis
References
Chapter 25 Separation and Spectroscopy of Paraffinic Hydrocarbons from Coal
I. Introduction
II. Extraction and Separation of Paraffinic Hydrocarbons from Coal and Coal Products
III. Subfractionation of Coal Paraffins
IV. Characterization of Alkanes by Gas Chromatography
V. Spectroscopic Examination of Coal Paraffins
VI. The Distribution of Paraffins in Coal and Coal Products
VII. Conclusion
References
Part VI Minerals in Coal
Chapter 26 Analysis of Mineral Matter in Coal
I. Introduction
II. Separation of Minerals from Coal
III. Analytical Procedures
References
Chapter 27 Separation and Identification of Minerals from Lignites
I. Background and Present Status of Information
II. Mineral Separation
III. Mineral Identification
IV. Suggested Procedures
References
Chapter 28 Procedures for Analysis of Respirable Dust as Related to Coal Workers Pneumoconiosis
I. Introduction
II. Measurement of Respirable Coal Dust Weight
III. Free Silica
IV. Trace Elements
V. Organic Components
VI. Other Methods
VII. Summary
References
Part VII Coal Carbonization Products: Coke, Pitch
Chapter 29 Analysis of Metallurgical Cokes
I. Introduction
II. Sampling and Sample Preparation
III. Chemical Analysis
IV. Physical Tests
V. Mechanical Properties
VI. Concluding Remarks
References
Chapter 30 The Formation and Properties of Anisotropic Cokes from Coals and Coal Derivatives Studied by Optical and Scanning Electron Microscopy
I. Introduction
II. The Formation and Properties of Anisotropic Cokes
References
Chapter 31 Optical Properties of Carbonized Vitrinites
I. Introduction
II. The Carbonization Process
III. Equipment and Methods
IV. The Response of the Optical Properties of Vitrinites to Carbonization
V. Discussion
VI. Conclusions
References
Chapter 32 Reactivity of Heat-Treated Coals
I. Introduction
II. Experimental Measurement of Reactivity
III. Selected Experimental Results
References
Chapter 33 Analysis of Coal Tar Pitches
I. Introduction
II. Methods of Pitch Production
III. Types of Pitches
IV. Fields of Application of Coal Tar Pitches
V. Solvent Analysis of Pitches
VI. Analysis and Testing of Coal Tar Pitches
References
Chapter 34 Analysis of Coal Tar Binders for Electrodes
I. Carbon Electrode Manufacture
II. Production of Coal Tar Pitch
III. Pitch Binder Properties
IV. Flow Properties of Carbon Paste
V. Evaluation of Test Electrodes
VI. Summary and Conclusions
References
Part VIII Coal Combustion Products
Chapter 35 Sampling and Analysis of Emissions from Fluidized-Bed Combustion Processes—Part 1
I. Introduction
II. Generic Fluidized-Bed Combustion Processes
III. A Phased Approach to Sampling and Analysis
IV. Selection of FBC Process Streams for Sampling and Analysis
V. Areas of Analytical Interest
References
Chapter 36 Sampling and Analysis of Emissions from Fluidized-Bed Combustion Processes—Part 2
I. Introduction
II. Sampling Program
III. Analytical Program
References
Chapter 37 Thermal Analysis of Coal and Coal Ashes
I. Introduction
II. Basic Principles of Thermal Analysis Methods: DTA, TG, and DTG
III. Preparing the Specimens for Analysis
IV. Thermoanalytical Methodology for Coals
V. Thermal Analysis of Coal Ashes
References
Index
- Edition: 1
- Published: January 28, 1979
- Imprint: Academic Press
- Language: English
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